Original Research Article
An investigation into fabrication and
characterization of direct reaction synthesized
Al-7079-TiC in situ metal matrix composites
S.V. Sujith
a,
*
, Manas Mohan Mahapatra
b
, Rahul S. Mulik
a
a
Department of Mechanical and Industrial Engineering, Indian Institute of Technology Roorkee, Uttrakhand 247667,
India
b
School of Mechanical Sciences, Indian Institute of Technology, Bhubaneswar, Odisha 751013, India
1. Introduction
During the past decade aerospace and automobile industries
are becoming more challenging due to the specific property
requirements where conventional alloy systems are not
sufficient. Attempts to improve the performance character-
istics of aluminum alloys with a high strength second phases
are required for high strength to weight ratio [1]. Metal matrix
composites (MMCs) incorporate a broad variety of metal
systems (e.g. titanium, aluminum, magnesium, copper and
nickel alloys) using various reinforcements in the form of
fibers (Al
2
O
3
, SiC, graphite), whiskers (SiC) and particulate
reinforcing phases (SiC, Al
2
O
3
, B
4
C, TiC, TIB
2
) [2,3]. High quality
a r c h i v e s o f c i v i l a n d m e c h a n i c a l e n g i n e e r i n g 1 9 ( 2 0 1 9 ) 6 3 – 7 8
a r t i c l e i n f o
Article history:
Received 28 May 2018
Accepted 11 September 2018
Available online
Keywords:
In situ
Reaction synthesis
Mechanical testing
Metallography
a b s t r a c t
The present study was attempted to highlight a novel direct reaction synthesis in which
traditional casting plus rapid solidification techniques were implemented to produce Al-
7079-TiC in situ composites with homogenous microstructure and improved dispersion
strengthening by the reinforcing phases. Casted samples were effectively characterized by
scanning electron microscopy followed by energy dispersive spectroscopy and X-ray dif-
fraction. Ingot metallurgy showed a homogenous distribution of TiC particles inside the
grain. This particle behavior acted as an excellent nucleation sites for the Al dendrites to
grow unvaryingly. TiC reinforcements have semi coherent relationship with a-Al matrix. It
was observed that eutectic boundary includes the second phases based on h (MgZn
2
) and Mg
(Zn, Cu, Al)
2
. Almost 90% of the in situ reinforced TiC were homogenously distributed along
the center of the grain. Thermal history conditions have shown an exothermic behavior
during casting. Experimental results revealed the evolution of TiC particles in super-heated
melt region, i.e. dissolution of titanium continued by reaction of titanium with diffused
carbon in the Al matrix to form TiC particles. Further they acted as nucleation sites for the a-
Al dendrites to grow homogenously. This study presents optimum process temperature for
the Al-TiC in situ synthesis.
© 2018 Politechnika Wroclawska. Published by Elsevier B.V. All rights reserved.
* Corresponding author.
E-mail addresses: sujithsv88@gmail.com (S.V. Sujith), manasfme@gmail.com (M.M. Mahapatra), rsm@iitr.ac.in (R.S. Mulik).
Available online at www.sciencedirect.com
ScienceDirect
journal homepage: http://www.elsevier.com/locate/acme
https://doi.org/10.1016/j.acme.2018.09.002
1644-9665/© 2018 Politechnika Wroclawska. Published by Elsevier B.V. All rights reserved.