IJSRST20723 | Accepted : 01 March 2020 | Published : 04 March 2020 | March-April-2020 [ 7 (2) : 68-74 ]
© 2020 | International Journal of Scientific Research in Science and Technology
IJSRST | Volume 7 | Issue 2 | Print ISSN: 2395-6011 | Online ISSN: 2395-602X
DOI : https://doi.org/10.32628/IJSRST20723
68
Design, Synthesis and Characterization of Some Novel benzamide derivatives
and it’s Pharmacological Screening
Akshay R. Yadav*, Shrinivas K. Mohite
Department of Pharmaceutical Chemistry, Rajarambapu College of Pharmacy, Kasegaon, Maharashtra, India
Corresponding author E-mail:- akshayyadav24197@gmail.com
ABSTRACT
The new series of substituted N-(phenylcarbamothioyl)benzamide derivatives (2a-2f) was designed,
development and synthesized by using conventional and microwave method. In present work six different
N-(phenylcarbamothioyl)benzamide were synthesized. Substituted benzoyl chloride is converted into
benzoyl isothiocyanate by esterification. Benzoyl isothiocyanate is converted into Substituted
(phenylcarbamothioyl)benzamide by treating with substituted aniline. Confirmation of the chemical
structure of the synthesized was substantiated by TLC, IR, 1H NMR, MS spectroscopy. Novel synthesized
compounds screened for their in vivo and in-vitro anti-inflammatory studies and compound 2f shows
promising anti-inflammatory activity.
Keywords: Benzamide, Microwave, Anti-Inflammatory Activity
I. INTRODUCTION
Benzamide used in medicinal as well as non-
medicinal activities in industry. Thiourea is organic
compound having sulphur with the general formula
(R1R2N)(R3R4N)C=S. Thiourea and urea derivatives
show a broad spectrum of biological activities as anti-
HIV, antiviral, HDL-elevating, antibacterial and
analgesic properties. Acyl thiourea derivatives are
well known for wide range of biological activities like
bactericidal, fungicidal, herbicidal, insecticidal action
and regulating activity for plant growth. Thiourea
derivatives are exceptionally versatile building blocks
for the synthesis of a variety of heterocyclic
compounds. Diaryl thioureas exhibit significant
antifungal activity against the plant pathogens. Acyl
thioureas are well known for their superior pesticidal,
fungicidal, antiviral, and regulating activity for plant
growth. Thiourea derivatives have attracted great
attention as versatile ligands in numerous applications.
Benzamide is an aromatic amide that consists of
benzene bearing a single carboxamido substituent.
Over 30 drugs containing this functionality are in
clinical use, including antihypertensive agent,
antibacterial, antiprotozoal, antifungal, anti-
inflammatory, nonpeptidic vasopressin receptor
antagonists and translation initiation inhibitors. Some
important benzamide derivatives used as carbonic
anhydrase inhibitors of commercial importance.
“Green chemistry” is defined as the synthesis, design,
development and application of chemical products to
reduces hazardous substances. The application of
green chemistry principles and practices renders
regulation, control, clean-up, and remediation of the
environment. Thus its benefits can be expressed in
terms of economic impact. Therapeutically active and
new drug constituents are needed for the treatment of
different diseases.