An IMDAF Cascade Approach Toward the Synthesis
of the Alkaloid (± )-Minfiensine
Carolyn A. Leverett, Gang Li, Stefan France, and Albert Padwa*
Department of Chemistry, Emory University, Atlanta, Georgia 30322
chemap@emory.edu
Table of Contents for Spectra
Page 3
1
H-NMR (400 MHz, CDCl
3
) of compound 18
Page 4
13
C-NMR (100 MHz, CDCl
3
) of compound 18
Page 5
1
H-NMR (400 MHz, CDCl
3
) of compound 19
Page 6
13
C-NMR (100 MHz, CDCl
3
) of compound 19
Page 7
1
H-NMR (400 MHz, CDCl
3
) of compound 21
Page 8
13
C-NMR (100 MHz, CDCl
3
) of compound 21
Page 9
1
H-NMR (400 MHz, CDCl
3
) of compound 22
Page 10
1
H-NMR (400 MHz, CDCl
3
) of compound 23
Page 11
13
C-NMR (100 MHz, CDCl
3
) of compound 23
Page 12
1
H-NMR (400 MHz, CDCl
3
) of compound 27
Page 13
13
C-NMR (100 MHz, CDCl
3
) of compound 27
Page 14
1
H-NMR (400 MHz, CDCl
3
) of compound 32
Page 15
13
C-NMR (100 MHz, CDCl
3
) of compound 32
Page 16
1
H-NMR (400 MHz, CDCl
3
) of compound 34
Page 17
13
C-NMR (100 MHz, CDCl
3
) of compound 34
Page 18
1
H-NMR (400 MHz, CDCl
3
) of compound 50
Page 19
13
C-NMR (100 MHz, CDCl
3
) of compound 50
Page 20
1
H-NMR (400 MHz, CDCl
3
) of compound 54
Page 21
13
C-NMR (150 MHz, CDCl
3
) of compound 54
Page 22
1
H-NMR (400 MHz, CDCl
3
) of compound 56
Page 23
13
C-NMR (100 MHz, CDCl
3
) of compound 56
Page 24
1
H-NMR (400 MHz, CDCl
3
) of compound 58
Page 25
13
C-NMR (150 MHz, CDCl
3
) of compound 58
Page 26
1
H-NMR (400 MHz, CDCl
3
) of compound 55
Page 27
13
C-NMR (150 MHz, CDCl
3
) of compound 55
Page 28
1
H-NMR (400 MHz, CDCl
3
) of compound 57
Page 29
13
C-NMR (100 MHz, CDCl
3
) of compound 57
Page 30
1
H-NMR (600 MHz, CDCl
3
) of compound 59
Page 31
13
C-NMR (150 MHz, CDCl
3
) of compound 59
Page 32
1
H-NMR (600 MHz, CDCl
3
) of compound 61
Page 33
13
C-NMR (150 MHz, CDCl
3
) of compound 61
Page 34
1
H-NMR (400 MHz, CDCl
3
) of compound 62
Page 35
13
C-NMR (100 MHz, CDCl
3
) of compound 62
1