ORIENTAL JOURNAL OF CHEMISTRY
www.orientjchem.org
An International Open Access, Peer Reviewed Research Journal
ISSN: 0970-020 X
CODEN: OJCHEG
2019, Vol. 35, No.(3):
Pg. 1244-1247
This is an Open Access article licensed under a Creative Commons license: Attribution 4.0 International (CC- BY).
Published by Oriental Scientific Publishing Company © 2018
Synthesis Study of Precursor Mixture of verdantiol, aurantiol
and lyrame Schiff Base and Its Characterization Using GC-MS
CANDRA IRAWAN
1
, DIAN ISLAMIYATI
1
, ANDITA UTAMI
1
*,
RIKA PERDANA PUTRI
2
and SINGGIH WIBOWO1
1
Department of Chemical Analysis, Politeknik AKA Bogor, Jalan Pangeran Sogiri,
Tanah Baru, Bogor 16154, Indonesia.
2
PT. Nilam Widuri Bogor, Jalan Raya Tlanjung Udik, Cibinong, Indonesia.
*Corresponding author E-mail: andita@kemenperin.go.id
http://dx.doi.org/10.13005/ojc/350347
(Received: April 29, 2019; Accepted: June 18, 2019)
ABSTRACT
A mixture of verdantiol, aurantiol, and lyrame based schiff base precursors has been
prepared by a simple condensation method. The mixture product has been characterized by gas
chromatography and mass spectrophotometer (GC-MS). The color of product has been compared
with the standard of the mentioned schiff base which was confirmed as yellow colored solution. The
lyrame was not detected and the verdantiol showed as the most obtained product.
Keywords: Schiff base, Mixture, GC-MS, Fragrance.
INTRODUCTION
Perfume is one of chemical products
which is used in daily life by men and women.
1
In its production process, raw materials such as
fragrances are needed.
2,3
Fragrances are pure aroma
oil or extracted oil from aroma compound which
has not been added by alcohol or other chemicals.
4
Therefore, the smell of these compounds is very
strong and the form is like an oil.
4
Raw material of
this natural aroma depends on the result of natural
products and weather condition. Consequently, many
perfume producers have been developing synthetic
aroma compound which can be easily produced
continuously.
5
Synthetic raw material are is used in the
production of aroma compounds is Schiff base.
Schiff base is an aldehyde- or ketone-like compound
in which the carbonyl group is replaced by an
azomethine or imine group.
6-8
The advantage of
using schiff base is its specific aroma characteristic
and long-lasting, hence it can improve the quality
of aroma compound.
9,10
There are several types of
schiff bases such as lilyantine, jasmea, verdantiol,
aurantiol, lyrame dan cyclantine.
11
Verdantiol,
aurantiol and lyrame are a popular schiff bases
which are used in the production of flower aroma
compounds.
12
In order to produce verdantiol, aurantiol
Brief Communication