d e n t a l m a t e r i a l s 2 8 ( 2 0 1 2 ) 349–359
Available online at www.sciencedirect.com
jo u rn al hom epa ge : www.intl.elsevierhealth.com/journals/dema
Physical, mechanical and rheological characterization of
resin-based pit and fissure sealants compared to flowable
resin composites
Sébastien Beun
a,b,c,∗
, Christian Bailly
b,c
, Jacques Devaux
b,c
, Gaëtane Leloup
a,b,c
a
Department of Dentistry and Stomatology, Cliniques Universitaires Saint-Luc, Université catholique de Louvain, Brussels, Belgium
b
Institute of Condensed Matter and Nanosciences – Bio & Soft Matter (IMCN/BSMA), Université catholique de Louvain,
Louvain-la-Neuve, Belgium
c
Center for Research and Engineering of Biomaterials (CRIBIO), Brussels, Belgium
a r t i c l e i n f o
Article history:
Received 1 February 2011
Received in revised form
18 July 2011
Accepted 1 November 2011
Keywords:
Pit and fissure sealants
Resin composites
Flowable
Viscoelasticity
Mechanical properties
Filler particles
a b s t r a c t
Objectives. The purpose of this study was to compare the mechanical and rheological prop-
erties of resin-based pit and fissure sealants to flowable resin composites in order to define
clinical indications based on these properties.
Methods. Eight flowable resin composites (Admira Flow, Filtek Supreme XT Flow, FlowLine,
Grandio Flow, Point-4 Flowable, Premise Flowable, Revolution Formula 2, X-Flow) and four
resin-based pit and fissure sealants (Clinpro, Delton FS
+
, Estiseal F, Guardian Seal) were
used in this study. Their filler weight content was measured by thermogravimetric analy-
sis. Mechanical properties were measured: dynamic and static moduli of elasticity, flexural
strength and Vickers microhardness. Rheological measurements were performed using a
dynamic oscillation rheometer.
Results. Flowable resin composites have by far better mechanical properties than pit and
fissure sealants, except for Delton FS
+
. All the materials tested are non-Newtonian, shear
thinning fluids. They all showed elasticity even at the lowest frequencies but elasticity differs
pretty much from one material to another.
Significance. : Resin-based pit and fissure sealants seem appropriate for preventive pit and
fissure sealing. For enlarged fissures, it can be assumed that flowable resin composites with
low elasticity at low frequency are more appropriate.
© 2011 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
1. Introduction
Although occlusal surfaces represent only 12.5% of the total
surfaces of the permanent dentition, they account for almost
50% of the caries in school children [1]. Tooth surfaces with pits
and fissures are thus extremely vulnerable to the development
∗
Corresponding author at: School of Dentistry and Stomatology, Cliniques Universitaires Saint-Luc – Université catholique de Louvain,
Av. Hippocrate 10/5721, B-1200 Brussels, Belgium. Tel.: +32 2 764 57 30.
E-mail addresses: Sebastien.Beun@uclouvain.be, s.beun@skynet.be (S. Beun).
of caries [2]. Pit and fissure sealants were introduced in the
1960s as an attempt to prevent occlusal dental caries. From
then, their effectiveness has been demonstrated several times
[3–5].
Three main types of materials are available as pit and fis-
sure sealants: glass ionomer cements, compomers and resins.
Since the retention rate of glass ionomer cements, as well as
0109-5641/$ – see front matter © 2011 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.
doi:10.1016/j.dental.2011.11.001