Supporting Information:
Hydroamination of Terminal Alkynes with
Secondary Amines Catalyzed by Copper:
Regioselective Access to Amines
Janet Bahri,
a,b
Rémi Blieck,
a
Bassem Jamoussi,
b
Marc Taillefer*
a
and Florian
Monnier*
a
a
École Nationale Supérieure de Chimie de Montpellier,
Institut Charles Gerhardt Montpellier CNRS UMR 5253, AM2N
8 rue de l'Ecole Normale 34296 Montpellier Cedex 05, France
b
Laboratoire de Chimie, Institut Supérieur d’Education et de Formation Continue, 43 Rue de la
Liberté, 2019, Le Bardo, Tunisia.
florian.monnier@enscm.fr ; marc.taillefer@enscm.fr
I- General experimental methods S1-S2
II- Typical procedures for the preparation of compounds 3a-3w and 7a-7w: S2-S3
III- Characterization of compounds 7a-7w S4-S38
I. General considerations
All reactions were performed in oven-dried 45x14.75 mm Screw tubes under an atmosphere
of argon. N-methyl-2-pyrrolidone (NMP) was distilled from P
2
O
5
and stored over activated
3Å molecular sieves under an argon atmosphere. CuCN stored in a dessicator cabinet and
S1
Electronic Supplementary Material (ESI) for ChemComm.
This journal is © The Royal Society of Chemistry 2015