INTERNATIONAL JOURNAL OF APPLIED ENGINEERING RESEARCH, DINDIGUL
Volume 2, No 2, 2011
© Copyright 2010 All rights reserved Integrated Publishing Association
RESEARCH ARTICLE ISSN - 0976-4259
419
Study of chemical, optical and structural properties of 120 MeV Ni
11+
ions
beam irradiated poly (ethylene terephthalate) film
Vijay Kumar
1
, Sonkawade R G
2
, Yasir Ali
1
, Dhaliwal A.S
1
1- Department of Physics, Sant Longowal Institute of Engineering and Technology Longowal
Distt. Sangrur, Punjab-148106, India
2- School of Physical Sciences, Babasaheb Bhimrao Ambedkar University (A Central
University) Rae Bareli Road, Vidya Vihar, Lucknow-226025, India
rgs22@rediffmail.com
ABSTRACT
We study the effect of 120 MeV Ni
11+
ions beam irradiations at various fluence ranging from
3x10
10
to 3x10
12
ions/cm
2
on the optical, chemical, and structural properties of poly (ethylene
terephthalate) (PET) polymer films. Irradiation on polymeric materials generally leads to a
formation of free radicals and ions, with secondary effects such as cross-linking as well as
chain scission. To confirm these effects various characterization techniques have been
explored viz. UV-Vis, X-ray diffraction (XRD), and Fourier Transforms Infrared (FTIR)
spectroscopy. Substantial decrease in optical band gap is observed with the increase of the
ion fluence. In the FTIR spectra nearly all bands were decreases due the degradation of the
molecular structure after irradiation. XRD measurements show the decrease of the main XRD
peak intensity, reflects the loss of crystallinity after irradiation. Moreover, crystallinity and
crystallite size changes with increasing fluence. The results will be discussed on the basis of
ion beam induced modifications.
Keywords: PET, Heavy ion irradiation, UV-Vis, XRD, FTIR
Nomenclature
PET = Poly (ethylene terephthalate)
XRD = X-ray diffraction
FTIR = Fourier Transforms Infrared
S
e
= Electronic energy loss
S
n
= Nuclear energy loss
L = Particle size
b = Full width at half maxima
X
c
% = Percentage of crystallinity
LET = Linear energy transfer
N = Number of carbon atoms
1. Introduction
As advanced technologies keep developing every day, there is a constant need for novel
materials with special properties and/or combinations of unique properties. In pursuit of
modified and improved properties of polymers, recent research trends reflect a sheer