Research Article Patil et al., 10(9-10): Sep/Oct, 2019:6364-6384]
CODEN (USA): IJPLCP ISSN: 0976-7126
© Sakun Publishing House (SPH): IJPLS
6364
INTERNATIONALJOURNALOFPHARMACY&LIFESCIENCES
(Int. J. of Pharm. Life Sci.)
Process Validation for Famciclovir
Vishal Patil*, Deepak Kumar Gupta, Raju Choukse and Rakesh Patel
School of Pharmacy, Dr. APJ Abdul Kalam University, Indore (M.P.) - India
Abstract
The project entitled "Process validation of Famciclovir 500 mg Tablets" was carried out at Macleods
Pharmaceuticals as the validation batch met the specification of tablets. Process validation study on three
consecutive batches, Batch No. A, B,and C of Famciclovir 500 mg. Tablets having batch size of 112500 tablets was
successfully completed and the manufacturing critical process parameters were validated of this transferred product
to show that the process was under control. The study includes the validation of critical steps of manufacturing such
as blending, compression, coating and container packing. It shall also establish the suitability of equipments and area
used for the production. The process of manufacturing was carried as per the approved batch manufacturing card.
The all process validation batches had been manufactured and validated in full compliance with cGMP requirement.
Key-words: Process validation, Famciclovir, GMPs.
Introduction
-"Process validation is establishing documented
evidence which provides a high degree of assurance
that a specific process will consistently produce a
product meeting its pre determined specifications and
quality characteristics."
[1]
Conducting process validation is not only a
regulatory requirement, but also makes a great deal of
sense from engineering as well as a business point of
view. It is evident that pharmaceutical companies that
are well versed in conducting process validation have
a competitive advantage over those who are not.
Process validation is required, in both general and
specific terms, by the Current Good Manufacturing
Practices regulations for finished pharmaceuticals, 21
CFR parts 210 and 211. A requirement for process
validation is set forth in general terms in sections
211.100 written procedures; deviations-which states,
in parts; "there shall be written procedures for
production and process control designed to assure
that the drug products have the identity, strength,
quality and purity; they purport or are represented to
posses". Several sections of cGMP regulations states,
validation requirement in more specific terms.
Excerpts from some of the sections are: Section
211.100 sampling and testing of in process materials
and drug products.
* Corresponding Author
E.mail: cemoon06@gmail.com
a) "Control procedures shall be established to monitor
the output and validate the performance of those
manufacturing process that may be responsible for
causing variability in the characteristics of in process
material and drug products." Section 211.113 control
of microbiological contamination
b) "Appropriate written procedures, design to prevent
microbiological contamination of drug products
purporting to be sterile, shall be established and
followed. Such procedures shall include validation of
any sterilization process."
The requirement of process validation is implicit in
the language of schedule M, Good manufacturing
practices regulation which states "To achieve the
objective, each licensee shall evolve methodology
and procedure which should be documented and kept
for reference and inspection".
Process validation is required by the medical device
GMP regulation, 21 CFR parts 820. Section 820.5
requires every finished device manufacturer to states:
"Prepared and implement a quality assurance
program that is appropriate to the specific device
manufactured". Section 820.3 states: "All activities
necessary to verify confidence in the quality of the
process used to manufacture a finished device".
A generally stated requirement for process validation
is contained in section 820.100, states: "Written
manufacturing specification and processing
procedure shall be established, implemented, and
controlled to assure that device conforms to its
original design or any approved changes in that
design". Validation is an essential element in the