Angewandte Chemie Polyoxometalates DOI: 10.1002/ange.200805792 Synthesis of Orthorhombic Mo-V-Sb Oxide Species by Assembly of Pentagonal Mo 6 O 21 Polyoxometalate Building Blocks** Masahiro Sadakane,* Keiko Yamagata, Katsunori Kodato, Keisuke Endo, Koshiro Toriumi, Yoshiki Ozawa, Tomoji Ozeki, Takuro Nagai, Yoshio Matsui, Norihito Sakaguchi, William D. Pyrz, Douglas J. Buttrey, Douglas A. Blom, Thomas Vogt, and Wataru Ueda* Zuschriften 3840 2009 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim Angew. Chem. 2009, 121, 3840 –3844