Microwave phase shifter with planar capacitors using strontium titanate films A. Kozyrev, A. Ivanov, O. Soldatenkov, E. Gol’man, A. Prudan, and V. Loginov St. Petersburg State Electrotechnical University Submitted May 18, 1999 Pis’ma Zh. Tekh. Fiz. 25, 78–83 October 26, 1999 A design of a microwave phase shifter based on a loaded microstrip line using planar SrTiO 3 capacitors as nonlinear elements is described. The microwave phase shifter at T =300 K demonstrated a continuous phase shift between 0 and 55 deg in the frequency range 8.6–9.0 GHz with a phase error not exceeding 5 deg. The quality parameter of the phase shifter in the operating frequency range was 110 deg/dB. © 1999 American Institute of Physics. S1063-78509902910-9 The nonlinear properties of ferroelectric materials such as strontium titanate SrTiO 3 and barium strontium titanate Ba,SrTiO 3 can be used to design electrically controllable microwave devices tunable resonators and filters, phase shifters, and so on. 1,2 Previous studies of ferroelectrics have demonstrated their high speed 3 and their capacity to operate at high microwave powers without any substantial degrada- tion of the dielectric properties. 4 Bearing in mind the rela- tively low cost of ferroelectric nonlinear elements compared with similar semiconducting and ferrite components, we note that these may be potentially useful for the microwave range. Ferroelectric nonlinear elements for microwave devices op- erating at room temperature are usually based on Ba,SrTiO 3 films. However, the fairly strong temperature dependence of the permittivity and the relatively high level of microwave dielectric losses in these materials 5 limit their application in the microwave range at T =300 K. Strontium titanate films are used at cryogenic temperatures ( T 77 K Ref. 2. Nevertheless, the nonlinearity of the permittivity of SrTiO 3 in high static electric fields was recently demon- strated by the authors of Refs. 6–8 at T =300 K and low frequencies. The present study demonstrates for the first time the use of SrTiO 3 films in electrically controlled microwave devices at T =300 K. Here we report results of an investiga- tion of the characteristics of a microwave phase shifter using planar SrTiO 3 capacitors. MICROWAVE PROPERTIES OF SrTiO 3 CAPACITORS Strontium titanate films were prepared by rf magnetron sputtering of a stoichiometric target in an 0.7 O 2 – 0.3 Ar at- mosphere at pressure P =4 Pa. The substrates for the planar capacitors were prepared using single-crystal sapphire ( r -cut. The substrate temperature ( T =700°Cwas kept constant during the film deposition process. After the re- quired thickness of SrTiO 3 film had been reached ( h =0.8 m, deposition ceased and the samples were cooled to room temperature at a rate of 10 deg/min. Before deposit- ing the SrTiO 3 film, platinum Ptelectrodes were formed on the substrate surface by photolithography. The gap between the electrodes was g =4 m. After the film had been depos- ited, the multilayer SrTiO 3 /Ptelectrodes of the planar capacitor/Al 2 O 3 system was annealed in air for 2 h at T =1050°C. The technology used to fabricate the multilayer structures containing a thin SrTiO 3 film was described in greater detail in Ref. 8. The nonlinearity and dielectric losses of the SrTiO 3 capacitors were estimated by a resonance technique 5 at frequency f 10 GHz and T =300 K. It was established that as the dc bias U b applied to the capacitors increased to U b =400 V, their capacitance decreased by a factor of 1.8. The Q factor of the capacitors Q 70 ( Q =1/tan , where tan are the dielectric lossesincreased slightly, by no more than 10%, with increasing bias. TOPOLOGY OF MICROWAVE PHASE SHIFTER The topology of the microwave phase shifter is shown in Fig. 1. Two parallel LC circuits containing planar ferroelec- tric capacitors are incorporated in a microstrip line ( Z 0 =50 ). The LC circuits are connected by a section of mi- crostrip line having a lower wave impedance ( Z 01 =40 ) which is required to improve the matching of the phase shifter with the external microwave circuits. The length of the microstrip line connecting the LC circuits is approxi- mately 3/4 near the central frequency f 8.8 GHz in the operating range of the phase shifter. The planar SrTiO 3 ca- pacitors C were placed in the gaps between the microstrip line and radial quarter-wave loops which ensure that the short-circuiting condition is satisfied for the microwave sig- nal in this design of phase shifter. The inductances Lwere sections of microstrip line having a wave impedance Z =50 and lengths less than /4 and were shorted with respect to the microwave signal using the radial quarter-wave loops. A dc bias U b is supplied to the planar capacitors via thin 10 msilver Agwires soldered to the radial loops and the microstrip line of the phase shifter. MICROWAVE CHARACTERISTICS OF PHASE SHIFTER The frequency dependences of the transmission coeffi- cient S 21 and the phase shift of the microwave phase shifter are plotted in Figs. 2a and 2b. The measurements were made at T =300 K. A dc bias U b = 0–400 V was ap- plied to the planar SrTiO 3 capacitors. At the central fre- quency of the operating range, the insertion losses of the TECHNICAL PHYSICS LETTERS VOLUME 25, NUMBER 10 OCTOBER 1999 836 1063-7850/99/25(10)/2/$15.00 © 1999 American Institute of Physics