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COMMENT
1802366 (1 of 2) ©
2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
What Defines a Perovskite?
Joachim Breternitz* and Susan Schorr*
DOI: 10.1002/aenm.201802366
2) The B-cation coordination needs to be octahedral (or distorted
octahedra)
3) The [BX
6
] octahedra need to be organized in an all-corner
sharing 3D network
The reason for these rules lies in the close relationship
between structure and properties. This is in the case of semi-
conductors predominantly the relationship between atomic and
electronic structure: Once the octahedra are no longer organ-
ized in a 3D network, the electronic properties will become sig-
nificantly anisotropic and are hence no longer comparable to
those of the original structure type. It is unfortunate that we
need to insist on the fact that the B-cations should be octahe-
drally coordinated, as we found examples in the literature,
where “perovskite” materials were made of isolated metal-halide
tetrahedra.
[7]
We do agree with the authors that compounds in
the elpasolite-type structure with a general formula of A
2
BB’X
6
could be understood as double perovskites, since the corner
sharing network of octahedra is still in place. As an example,
we would like to highlight that structures in the K
2
PtCl
6
-type,
such as Cs
2
SnI
6
should by no means be understood as perovs-
kites. While Jodlowski et al. clearly state that the K
2
PtCl
6
struc-
ture type is composed of isolated [BX
6
] octahedra, they base
their reasoning for its categorization as perovskite on two main
points
[1]
: 1) the proximity of the [BX
6
]
2-
octahedra and 2) “the
vacancy-ordered double perovskites experience the same loss
of symmetry in phase transitions upon cooling as that occur-
ring in ABX
3
.”
[1]
Unfortunately, we are unable to agree to both
of these points: 1) the closest inter-octahedral I–I distance in
Cs
2
SnI
6
, for instance, is 4.18 Å,
[8]
which is significantly longer
than twice the corresponding van-der-Waals radius of iodine
(2·1.98 Å = 3.96 Å)
[9]
and hence no bonding would be expected
between the isolated octahedra. 2) The fact the K
2
PtCl
6
-type
structures show symmetry reduction upon cooling is nothing
that is mutually unique with the perovskite-type structures but
it is rather a general effect that low temperature phases are of
lower symmetry than high-temperature phases.
Analogous to the above-mentioned case, neither of the struc-
ture types further discussed in the paper obeys a 3D network of
corner sharing octahedra (or distorted octahedra) and therefore
cannot be regarded as of perovskite-type. In particular for the
Ruddlesden–Popper phases, we would like to draw the attention
of the reader to the original publications of Ruddlesden and
Popper,
[10,11]
where the authors point out that these compounds
contain perovskite layers. Perovskite layers are, however, not
layered perovskites and no matter how small the change in
semantics may appear, the latter would not be correct.
Finally, we do understand the incentive of the research
community to rationalize this category of materials under a
common naming and do believe that this facilitates the discus-
sion amongst the research community. With the reasoning laid
out above, however, we do not believe that the term “perovskite”
is appropriate for all of the materials but should only be used
Dr. J. Breternitz, Prof. S. Schorr
Helmholtz-Zentrum für Materialien und Energie
Structure and Dynamics of Energy Materials
14109 Berlin, Germany
E-mail: joachim.breternitz@helmholtz-berlin.de;
susan.schorr@helmholtz-berlin.de
Prof. S. Schorr
Department Geosciences
Freie Universität Berlin
Berlin 12249, Germany
The ORCID identification number(s) for the author(s) of this article
can be found under https://doi.org/10.1002/aenm.201802366.
After reading the recent publication of Jodlowski et al.
[1]
with
great interest, we would like to address a misconception, that
is unfortunately common in the field. Jodlowski et al. give a
great and comprehensive overview over the different possibili-
ties of overcoming the intrinsic problems of lead based halide
perovskite semiconductor materials, including cation and
anion substitutions.
[1]
The fundamental problem, however, lies
in the use of the term “perovskite” for all of these structures.
The perovskite structure type is a clearly defined term that
should be used in its correct way, and we would like to urge the
research community to obey these rules.
In order to define the term perovskite properly, one should
note the following fact: The mineral named perovskite, CaTiO
3
,
was first described by Rose, a German mineralogist who
described the habit and some reactions of what he named
perovskite after Russian mineralogist Lev Perovski.
[2]
We
would argue that materials that can be counted to this struc-
tural family should exhibit a close structural similarity to the
crystal structure of the defining mineral Perovskite (CaTiO
3
)
and some criteria for this are given below. It might be, that
some of the confusion could stem from the fact that at ambient
conditions, CaTiO
3
itself does not crystallize in the cubic aristo-
type structure, but rather in an orthorhombic structure which
can be derived from the cubic aristotype in a group-subgroup
relationship.
[3]
Generations of crystallographers and solid state
chemists have dedicated their work to the elucidation of the
structural relations between the cubic aristotype of the pero-
vskite type structure and its many lower symmetry variations
(hettotypes).
[4]
In fact, the perovskite type is one of the classical
examples for the use of group–subgroup relationships and
we would like to highlight the work of Bock and Müller
[5]
and
Bärnighausen
[6]
on the thorough understanding and rationali-
zation of these structural relationships and ultimately, a pero-
vskite needs to adopt a crystal structure of the perovskite aristo-
type or a hettotype thereof.
From our point of view, three major points must be obeyed
for a material to be called a perovskite:
1) A stoichiometry of ABX
3
, or at least a ratio A:B:X of 1:1:3
Adv. Energy Mater. 2018, 8, 1802366