Surface and Coatings Technology, 36 (1988) 939 -947 939
A NEW TYPE OF TRANSDUCER FOR PARTIAL PRESSURE
CONTROL*
C. A. GOGOL and R. MUELLER
Leybold Inficon Inc., 6500 Fly Road, East Syracuse, NY 13057 (U.S.A.)
(Received April 12, 1988)
Summary
A new transducer for controlling the partial pressure of sputtering gases
is described. Utilizing the electron impact emission spectroscopy (EIES)
principle, an instrument capable of operating in a total pressure environ-
ment of 100 X iO~ Torr or more with minimum detectable partial pressures
to 10’ Torr is described. These capabilities seem ideal for controlling
reactive deposition processes utilizing N
2, 02 or hydrocarbons. Because of
the high operating pressure capabilities, this transducer does not require the
complication of high vacuum pressure reduction and thus eliminates a major
source of unscheduled maintenance.
The operating principles of EIES and the sensitivities that were de-
termined for the various gases tested are described in this paper. The present
authors have found the technique to have high stability over extended
periods of time (about ± 3.5% over 30 days) and sufficient sensitivity to
control processes of present practical interest. In addition to the use for
direct partial pressure control the technique has utility for monitoring
common residual gases such as H20 and CO2. in an analyzer mode, as a pre-
cursor to starting the reactive process.
1. Introduction
Over the past several years the present authors have been developing a
new technology for partial pressure analysis and control. This technology,
based on electron impact emission spectroscopy [1, 2] has a set of unique
properties and advantages for the intended applications, e.g. partial pressure
control of reactive high rate sputtering [3] and low vacuum gas analysis.
Specifically, the advantages are perceived to be as follows.
(A) Stability: a long-term constancy far exceeding that demonstrated
by other instruments used today.
(B) Simplicity: a design that requires no moving parts, no critical
voltages and no close tolerances. These all combine to make for an instru-
*paper presented at the 15th International Conference on Metallurgical Coatings,
San Diego, CA, U.S.A., April 11 - 15, 1988.
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