Supporting Information
for
The first examples of multiply bonded dirhenium(III,II)
paramagnetic complexes that contain nitrobenzoate ligands:
spectroscopic, structural, cytotoxicity and computational studies†
Suman Mallick,
a
Mrinal Kanti Ghosh,
a
Suman Mandal,
a
Vinayak Rane,
b
Ramakant
Kadam,
b
Annesha Chatterjee,
c
Arindam Bhattacharyya
c
and Swarup Chattopadhyay*
,a
a
Department of Chemistry, University of Kalyani, Kalyani, Nadia 741235, WB, India. Tel.:
+91 33 25828750; Fax: +91 33 25828282. E-mail: icskc@klyuniv.ac.in (S. Chattopadhyay)
b
Radiochemistry Division, RLG, Bhabha Atomic Research Centre, Mumbai 400085, India
c
Immunology Laboratory, Department of Zoology, University of Calcutta, 35 Ballygunge
Circular Road, Kolkata – 700019, India
Contents of Supporting Information
Fig. S1 Solid state powder X-band EPR spectrum of 2 at 298 K
Fig. S2 Solid state powder X-band EPR spectrum of 3 at 298 K
Fig. S3 Solid state powder X-band EPR spectrum of 4 at 298 K
Fig. S4 X-Band EPR spectrum of dichloromethane glass of 2 recorded at 126 K
Fig. S5 X-Band EPR spectrum of dichloromethane glass of 3 recorded at 126 K
Fig. S6 Isodensity plot of spin-up frontier molecular orbitals of 2, 3, 4 and the model Re
2
(μ-
O
2
CC
6
H
4
)Cl
4
(μ-dppm)
2
complex
Fig. S7 Growth inhibitory effect of the nitrobenzoic acid ligands on MCF-7 cells.
Fig. S8 Growth inhibitory effect of the acetate and benzoate complexes on MCF-7 cells.
Electronic Supplementary Material (ESI) for Dalton Transactions.
This journal is © The Royal Society of Chemistry 2017