Proceedings of the Pakistan Academy of Sciences 48 (2): 95–100, 2011 Pakistan Academy of Sciences
Copyright © Pakistan Academy of Sciences
ISSN: 0377 - 2969
Original Article
Preparation and Evaluation of Clotrimazole Matrix Type Patch:
Effect of Olive Oil on Drug Penetration Across Rabbit Skin
Asif Nawaz, Gul Majid Khan, Shefaat Ullah Shah
*
, Kifayat Ullah Shah,
Asim-ur-Rehman and Abid Hussain
Department of Pharmaceutics, Faculty of Pharmacy, Gomal University,
Dera Ismail Khan, K.P.K., Pakistan
Abstract: The present study was conducted to formulate and evaluate transdermal patch of
Clotrimazole for local as well as systemic therapy of severe to moderate fungal infections. The
penetration effect of naturally occurring oil [Olive oil] was investigated on the in vitro penetration
enhancement of Clotrimazole across synthetic membrane as well as albino rabbit skin. Clotrimazole
was evaluated for its particle size and particle size distribution analysis by using Particle size analyzer
[Horiba LA 300]. Clotrimazole patches were formulated by solvent evaporation method for in vitro
drug penetration studies. Olive oil was added to some selected formulations at different concentrations
i.e. 0.5, 1, 1.5, 2, 2.5 and 3% to see their effect on drug release patterns.The formulated patches were
evaluated for various physico-chemical parameters to check their suitability for topical application.
Franz diffusion cell Apparatus [Perm Gear, USA] was used for in vitro drug release studies having
phosphate buffer pH 7.4 as receptor solvent.
Keywords: Clotrimazole; transdermal patch; Franz diffusion cell; olive oil.
NTRODUCTION
The transdermal drug delivery system is oftenly
comprised of low bioavailability of the drug
because of the barrier functions of the skin [1],
but the drug release from this route is constant
because of the avoidance of first-pass
metabolism by the GIT. The amount of drug
required for therapeutic effect in transdermal
drug delivery systems as compared to oral routes
is less bioavailable but the amount available is
sufficient for therapeutic uses [2]. Transdermal
drug delivery systems are used to treat several
diseases but with limitations due to poor
penetration through the skin. Topical
formulations like creams, ointments,gels and
patches can improve the delivery of certain
drugs; this fact could be of great importance in
succeeding the transdermal therapeutic
approaches. The goal of improving the
penetration of certain drugs via transdermal
route can be achieved through penetration
enhancers [3]. The poor absorption of the drug
could be presumed by its physico-chemical
properties but the drug’s penetration can be
enhanced by the modification of medicinal
chemists and nature of physiological barriers. To
overcome the physiological barriers great
investigative studies have been carried out by
scientists so far and came to know that
penetrative properties of drugs via transdermal
route could be enhanced by using certain natural
and synthetic compounds [2]. The use of certain
systems that has greater chemical potential then
that of corresponding saturated solutions is an
alternative method and also that can promote the
penetration of the drug from vehicle to the skin.
Transdermal patches proved the efficacy of such
studies. Drug loaded monolayer transdermal
patch can be easily prepared by fast solvent
evaporation [1].
MATERIAL AND METHODS
Clotrimazole (Leads Pharma Islamabad,
Pakistan), Carboxy polymethylene (Sigma
Chemicals, USA), Triethanolamine, PVP K30
(Merk, Germany), Ethyl cellulose, Polyethylene
glycol 400, Potassium dihydrogen phosphate,
Sodium hydroxide (Merk, Germany), Ethanol,
Olive oil [Sigma Aldrich, Germany], Magnetic
stirrer, pH meter, Weighing balance, UV-Visible
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Received May 2011, Accepted June 2011
*
Corresponding Author: Shefaat Ullah Shah; Email: kifayat83@yahoo.com