materials
Review
Dendrimeric Structures in the Synthesis of Fine Chemicals
Bruno Mattia Bizzarri * , Angelica Fanelli, Lorenzo Botta , Claudio Zippilli, Silvia Cesarini
and Raffaele Saladino *
Citation: Bizzarri, B.M.; Fanelli, A.;
Botta, L.; Zippilli, C.; Cesarini, S.;
Saladino, R. Dendrimeric Structures
in the Synthesis of Fine Chemicals.
Materials 2021, 14, 5318. https://doi.
org/10.3390/ma14185318
Academic Editor: Ivo Grabchev
Received: 21 July 2021
Accepted: 9 September 2021
Published: 15 September 2021
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Biological and Ecological Sciences Department (DEB), University of Tuscia, 01100 Viterbo, Italy;
fanelli.angelica@gmail.com (A.F.); lorenzo.botta@unitus.it (L.B.); zippillic@unitus.it (C.Z.);
c.cesarinisilvia@gmail.com (S.C.)
* Correspondence: bm.bizzarri@unitus.it (B.M.B.); saladino@unitus.it (R.S.)
Abstract: Dendrimers are highly branched structures with a defined shape, dimension, and molecular
weight. They consist of three major components: the central core, branches, and terminal groups.
In recent years, dendrimers have received great attention in medicinal chemistry, diagnostic field,
science of materials, electrochemistry, and catalysis. In addition, they are largely applied for the
functionalization of biocompatible semiconductors, in gene transfection processes, as well as in the
preparation of nano-devices, including heterogeneous catalysts. Here, we describe recent advances
in the design and application of dendrimers in catalytic organic and inorganic processes, sustainable
and low environmental impact, photosensitive materials, nano-delivery systems, and antiviral
agents’ dendrimers.
Keywords: dendrimers; heterogenous catalysis; materials; PAMAM; nano-devices; anti-virals
1. Introduction
Dendrimers are symmetric and monodisperse macromolecules with a well-defined three-
dimensional branched shape inspired by that of a tree [1]. They show three topologically
different regions including: (i) the core part; (ii) the branches formed by repetitive monomeric
units (dendrons); and (iii) the “periphery” as final appendages of the dendrons [2]. Two
different synthetic methodologies are commonly used for the preparation of dendrimers:
(a) the divergent approach, in which dendrimers grow from the core proceeding radially
outward toward the periphery; (b) the convergent one, in which the growth starts from
the periphery of the dendrimer toward the inner part. The choice of the specific synthetic
approach is usually related to the desired application field, depending on both the target
chemical structure (sequence of dendrons and order of generation) and the building
blocks selected for the construction of the dendritic framework. Dendrimers are classified
according to the ‘generation’ level, which represents the minimum number of branching
nodes from the core to the periphery. These systems are highly ordered three-dimensional
structures often characterized by internal cavities in which metal ions and small molecules
can be hosted [3,4].
2. Application of Dendrimers in the Science of Materials Field
Dendrimers represent a potent tool in the design of novel sustainable and low envi-
ronmental impact materials, as optimal reagents, or, alternatively, as structural components
in the preparation and functionalization of advanced fibers and composites. For example,
they can solve pollution problems associated with the dyeing of cellulose fibers, usually
performed with high amounts of electrolyte and alkali solutions [5]. The application of
poly-amidoamine (PAMAM) dendrimers modifies the surface of cotton fibers, increasing
the dye uptake and fixation without the use of toxic substances [6]. The PAMAM treat-
ment introduces nucleophile amino groups in the polysaccharide able to capture dyes
without the use of electrolytes and alkali, minimizing the dye hydrolysis, and reducing
Materials 2021, 14, 5318. https://doi.org/10.3390/ma14185318 https://www.mdpi.com/journal/materials