Volume 3 • Issue 1 • 1000112
J Nanomedine Biotherapeutic Discov
ISSN:2155-983X JNBD an open access journal
Research Article Open Access
Nanomedicine & Biotherapeutic
Discovery
Konstantinović et al., J Nanomedine Biotherapeutic Discov 2013, 3:1
http://dx.doi.org/10.4172/2155-983X.1000112
Keywords: Self-assembled nanostructures; Magnetoresistance;
Oxide surfaces; Spintronics
Introduction
e recent idea of using biomolecules with magnetic particles
as magnetic markers in living organisms opens the door to a new
generation of magnetoresistive detectors with sensitivity over the
standard detection by fluorescence [1,2]. is technology is based on
the detection of nanometric magnetic labels biologically functionalized
by ultra-sensitive magnetic field microsensors due to the change in
the resistance. Resistive devices, based on the giant magnetoresistive
(GMR) or tunnel magnetoresistive (TMR) effects, have been intensively
studied in the emerging field of spintronics [3,4]. Nowadays, magnetic
junctions are key components in several commercial products in
different areas and recently have been used in new types of test of
biomolecular systems with integrated recognition [5-7]. Moreover, a
huge increase of tunnelling magnetoresistance has been observed in
TMR nanometric junctions based on metallic nanoparticles. Well-
defined structures at nanometric scale present an increasing interest
due to their unique physical properties allowing envisaging new
technological applications. In particular, the large surface to volume
ration in nanoparticulate systems holds very promising expectatives in
catalysis.
A major challenge in nanotechnology is to find a way of positioning
nanoelements on surfaces in regular patterns, with nanometric precision
yet over large surface areas either by deposition techniques (bottom-up
approach) or by lithography plus nanofabrication techniques (top-
down approach). Fabrication of artificial nanostructures of oxide
materials by top-down approach requires sophisticated technology
and has been recognized as a hard-attainable issue. For these reasons,
the fabrication of ordered nanostructures, via spontaneous self-
organization, is a topic of major relevance. An attractive route is based
on using self-assembly properties of basic building blocks to create the
patterned nanostructure. In this sense, directed self-organization based
on template-assisted processes is a very promising and fast developing
research topic in different fields.
e tendency of some oxides towards self-organized growth,
forming regular arrays of 3D uniform structures, offers enormous
potential for the preparation of nanotemplates that can be used for the
fabrication of long range ordered nanostructured systems [8].
In this article, we explore the possibility of using long range
ordered arrays of nanoobjects, obtained by spontaneous self-assembly
in epitaxial La
0.7
Sr
0.3
MnO
3
(LSMO) thin films, as nanostencils for
fabricating arrays of metallic nanoparticles (sub-50 nm range) prepared
by physical and chemical methods. e preparation of Au nanoparticles
arrays by a self- organization process guided by the nanostructured
surface morphology of the underlying LSMO is demonstrated to
illustrate the suitability of the method.
Materials and Methods
LSMO thin films were grown on (001)-oriented SrTiO
3
substrates
by rf magnetron sputtering from a stoichiometric ceramic target [9].
e crystal structure was characterized by X-ray diffraction (XRD)
with Cu Kα radiation. Pole figure has been recorded using a Bruker
AXS GADDS system equipped with a 2D X-ray detector. e surface
morphology was analyzed by atomic force microscopy (AFM) working
*Corresponding author: Konstantinović Z, Institut de Ciència de Materials de
Barcelona, CSIC, Campus UAB 08193, Bellaterra, Spain; E-mail: zorica@icmab.es
Received June 01, 2013; Accepted June 24, 2013; Published June 27, 2013
Citation: Konstantinović Z, Vodnik V, Saponjic Z, Nedeljkovic J, Pomar A, et
al. (2013) Self-Assembled Nanostructures as Templates for the Integration of
Nanoparticles in Oxide Surfaces. J Nanomedine Biotherapeutic Discov 3: 112.
doi:10.4172/2155-983X.1000112
Copyright: © 2013 Konstantinović Z, et al. This is an open-access article
distributed under the terms of the Creative Commons Attribution License, which
permits unrestricted use, distribution, and reproduction in any medium, provided
the original author and source are credited.
Self-Assembled Nanostructures as Templates for the Integration of
Nanoparticles in Oxide Surfaces
Konstantinović Z
1
*, Vodnik V
2
, Saponjic Z
2
, Nedeljkovic J
2
, Pomar A
1
, Santiso J
3
, Sandiumenge F
1
, Balcells Ll
1
and Martinéz B
1
1
Institut de Ciència de Materials de Barcelona, CSIC, Campus UAB 08193, Bellaterra, Spain
2
Vinča Institute of Nuclear Sciences, P.O. Box 522, 11001 Belgrade, Serbia
3
Centre for Nanoscience and Nanotechnology, (CSIC-ICN) Campus UAB, 08913 Bellaterra, Spain
Abstract
Under properly selected growth conditions, complex oxide thin films might exhibit a tendency towards self-
organization allowing obtaining regular arrays of three-dimensional nanostructures. This behavior, together with
their rich physics, offers enormous potential for the implementation of new nanodevices. Among complex oxides,
manganese perovskites exhibiting colossal magnetoresistance and half-metallic character have emerged as
promising candidates for the implementation of new spintronic devices.
Manganite thin films are often elastically strained, due to film-substrate lattice mismatch, and this lattice
strain can, in some cases, select preferential growth modes leading to the appearance of different self-organized
nanostructured morphologies. It is shown that under properly chosen growth conditions long range ordered arrays
of nanoobjects, running along the steps direction defined by the miscut angle of the underlying substrate, can be
obtained in highly epitaxial La
2/3
Sr
1/3
MnO
3
(LSMO) thin films. These results suggest that self-organization process
is directly guided by the topological features of the underlying substrate and highlight the relevance of growth
kinetic effects. The use of those nanoobjects arrays as nanostencils for fabricating arrays of nanoparticles is also
explored.