RESEARCH ARTICLE
Nanoporous hierarchical carbon structures derived from fungal
basidiocarps for high performance supercapacitors
Krishna Prasad Gannavarapu
1
| Samar Azizighannad
2
| Muralikrishna Molli
3
|
Meera Pandey
4
| Sai Muthukumar V
3
| Somenath Mitra
2
| Rajesh Babu Dandamudi
1
1
Department of Chemistry, Sri Sathya Sai Institute of Higher Learning, Prasanthi Nilayam Campus Puttaparthi, Anantapur District, Andhra Pradesh, India
2
Department of Chemistry and Environmental Science, New Jersey Institute of Technology, Newark, New Jersey
3
Department of Physics, Sri Sathya Sai Institute of Higher Learning, Prasanthi Nilayam Campus Puttaparthi, Anantapur District, Andhra Pradesh, India
4
Department of Plant Pathology, Indian Institute of Horticultural Research, Hessaraghatta Lake Post, Bangalore, Karnataka, India
Correspondence
Rajesh B. Dandamudi, Department of
Chemistry, Sri Sathya Sai Institute of Higher
Learning, Prasanthi Nilayam Campus
Puttaparthi, Anantapur District,
Andhra Pradesh 515134, India.
Email: drajeshbabu@sssihl.edu.in
Somenath Mitra, Department of Chemistry
and Environmental Science, New Jersey
Institute of Technology, 151 Tiernan Hall,
Newark, NJ 07102.
Email: somenath.mitra@njit.edu
Funding information
Department of Science and Technology,
Ministry of Science and Technology, Grant/
Award Number: SR/FST/PSI-172/2012;
National Institute of Environmental Health
Sciences, Grant/Award Number:
R01ES023209
Abstract
This article presents the first report on systematic synthesis and evaluation of acti-
vated carbons from the cap and stalk of two diverse mushroom species namely,
Ganoderma lucidum (GL) and Calocybe indica (CI) belonging to different classes
white rot and brown rot respectively. A novel microwave induced H
3
PO
4
activation
followed by carbonization and KOH activation enabled the formation of activated
carbon with hierarchical structures. The activated carbons from cap and the stalk of
the mushrooms are different in terms of specific surface area, pore volume, and
their electrochemical behavior. Specific surface area and pore volume from GL-cap
is as high as 2432.4 m
2
/g and 0.54 CC/g, respectively. After optimization, the acti-
vated carbons have high graphitic content, good thermal stability and show specific
capacitance as high as 271.94 F/g, energy and power densities of 13.59 Wh/kg and
127.31 W/kg, respectively. All the carbons show good capacitance retention up to
10 000 cycles. The surface area and specific capacitance in the mushroom stalks are
lower than the ones made from the caps and the highest surface area and specific
capacitance are 1576.2 m
2
/g and 137.2 F/g respectively for GL-stalk.
KEYWORDS
activated carbon, Calocybe indica, Ganoderma lucidum, hierarchical porous structures, mushrooms,
super capacitance
1 | INTRODUCTION
The physical and chemical properties of activated carbon
(AC) such as porosity, surface area, and surface chemistry
are important considerations for different applications.
1
Com-
mercially available ACs are traditionally made from synthetic
polymers to achieve hierarchical structuring
2
or from plant
materials like coconut shell.
3
These have been used as sorbents
for heavy metals
4
and dyes,
5
as capacitor electrodes,
6
and as
solid supports for catalysts.
7
The precursor as well as the
physical/chemical processes in synthesis and activation steps
play major roles in determining the characteristics and proper-
ties of the resulting AC, which can be microporous, meso-
porous, or macroporous.
8
ACs have been traditionally derived from high temperature
carbonization of both natural and synthetic polymers.
9
Among
Received: 5 April 2019 Revised: 29 April 2019 Accepted: 29 April 2019
DOI: 10.1002/est2.58
Energy Storage. 2019;1:e58. wileyonlinelibrary.com/journal/est2 © 2019 John Wiley & Sons, Ltd. 1 of 12
https://doi.org/10.1002/est2.58