SPECTROCHIMICA
ACTA
PART B
ELSEVIER Spectrochimica Acta Part B 52 (1997) 1377-1394
Adaptation of the filter furnace atomizer for atomic absorption
determination of less volatile metals 1
D.A. Katskov a'*, P.J.J.G. Marais a, V.J. Katkovnik b, P. Tittarelli c
~Department of Chemistry and Physics, Technikon Pretoria, Private Bag X680, Pretoria, South Africa
bDepartment of Statistics, University ~ South Africa, PO Box 392. Pretoria, South Africa
~Stazione Sperimentale per i Combustibili, Viale A. De Gasperi 3. 20097 San Donato Milanese, MI, ltalv
Received 30 July 1996; accepted 22 October 1996
Abstract
The filter furnace atomizer (FF), which has already been proposed for electrothermal atomic absorption spectrometry,
provides enhanced sensitivity, a reduction of interferences and reduced analytical time. The main disadvantage of the FF is
the rapid destruction of the filter at the atomization temperatures of less volatile or carbide-forming elements. In the current
work, radiative heat exchange between the components of the FF was considered to be predominant at high temperature. The
thermal behaviour of the FF was therefore examined at fast heating rate as a function of its configuration, the type of graphite
used for the components, and the voltage applied. The optimal combination of electrical resistivity, relative dimensions and
mass of the FF components was determined for the HGA-500 atomizer. The improvements resulted in a significantly increased
lifetime of the FF in the multiple determination of Al, As, Co, Cr, Cu and Ni. The filter withstood 150 firings at 2600°C (hold
time 15 s) in the determination of Cr. The theoretical approach can be applied to different types of atomizers. © 1997 Elsevier
Science B.V.
Keywords: Electrothermal atomic absorption spectrometry; Filter furnace; Heat exchange; Matrix interference minimization;
Theoretical modelling
1. Introduction
The main advantages of the filter furnace (FF), a
new atomizer for electrothermal atomic absorption
spectrometry (ET AAS), are the increase of the
sampling volume up to 100/zl, the short drying period
(10-15 s), a two- to threefold improvement in
detection limit, and efficient reduction of background
and chemical interferences [1-5]. The general design
of the FF is displayed in Fig. 1(a).
~ Presented at the Second European Furnace Symposium, St.
Petersburg, Russia, May 1996.
* Corresponding author.
Liquid samples are dispensed into the ring cavity
between the pyrocoated tube 1 and the filter 2 (made
of porous graphite), dried, ashed and atomized in
accordance with the appropriate program. After dry-
ing, fine particles of the residue are scattered over the
fibre 3. During the atomization stage the sample
vapours enter the analytical zone in the central part
of the filter through the pores of the graphite.
The advantages of the FF are fully displayed during
the evaporation of volatile elements and matrices that
do not form stable chemical compounds or solid solu-
tions with graphite. The configuration of the filter and
its material were chosen empirically to reach low
detection limits [5]. The goal of that FF design was
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