FEMS MicrobiologyLetters 83 (1991) 29-34
© 199l Federation of European Microbiological Societies 0378-1097/91/$03.50
Published by Elsevier
ADONIS 037810979100406S
29
FEMSLE 04601
High level production of Echerichia coli outer membrane
proteins OmpA and OmpF intracellularly in Bacillus subtilis
Ritvaleena Puohiniemi, Sarah Butcher, Eveliina Tarkka and Matti Sarvas
National Public Health Institute, Helsinki, Finland
Received 6 June 1991
Accepted 11 June 1991
Key words: OmpA production; Escherichia coli; OmpF production; Bacillus subtilis;
Outer membrane proteins; Inclusion bodies; Detergent solubilization
1. SUMMARY
A high yield of Escherichia coli outer mem-
brane proteins OmpA (about 200 mg/1) and
OmpF (about 100 rag/l) was obtained in Bacillus
subtilis when produced intracellularly. The yield
was more than 100-fold higher than the yield of
these proteins by a similar vector containing the
complete signal sequence of a-amylase of B.
amyloliquefaciens. Both proteins isolated after
breakage of the B. subtilis cells by low-speed
centrifugation were about 70% pure and could be
solubilized by Sarkosyl, SDS and guanidine hy-
drochloride.
2. INTRODUCTION
Outer membrane proteins of Gram-negative
bacteria have been a subject of considerable in-
terest as potential vaccine candidates and as anti-
Correspondence to." R. Puohiniemi, National Public Health
Institute, Mannerheimintie 166, SF-00300 Helsinki, Finland.
gens for immuno-diagnosis. For these purposes
large quantities of purified proteins would be
needed, a goal made difficult by their nature as
integral membrane proteins and their tight asso-
ciation with other outer membrane components,
especially endotoxin (lipopolysaccharide, LPS)
(see review [1]). Producing them in a heterolo-
gous organism which lacks both the outer mem-
brane and LPS therefore would offer many ad-
vantages.
We have recently described the use of the
Gram-positive Bacillus subtilis as a host for the
synthesis of the outer membrane protein OmpA
of Escherichia coli [2,3]. However, the production
level obtained was relatively low, about 1 mg/l of
culture. In those studies we used an expression
and secretion vector which contained the efficient
a-amylase promoter of B. amyloliquefaciens fol-
lowed by the secretory signal sequence of the
same gene. The OmpA expressed from this vec-
tor was cell-associated, not secreted, and the sig-
nal sequence was not cleaved [2,3].
In this paper we examine the possibility of
obtaining a higher yield of OmpA in B. subtilis by
deleting the signal sequence and thus directly
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