Synthesis of Nanopowders and Consolidation of Nanoceramics of
Various Applications
Edwin Gevorkyan
1
, Dmitry Sofronov
2
, Sergiy Lavrynenko
3*
and Miroslaw Rucki
4
1
Ukrainian State University of Railway Transport, Kharkov, Ukraine
2
State Scientific Institution “Institute for Single Crystals” National Academy of Sciences of Ukraine
3
National Technical University “Kharkov Polytechnic Institute”, Ukraine
4
Kazimierz Pulaski University of Technology and Humanities in Radom, Poland
Email: s_lavr@yahoo.com
Abstract. In the paper, some problems of nanoceramics production are discussed. Some crucial
stages in the production cycle are pointed out, among others the nanoscale powder synthesis and the
compaction during the sintering. A novel method of hot pressing under the directly applied electric
current was proposed. Some examples of advantageous characteristics obtained through the new
method were provided. The hot press sintering under the electric current is suitable for the
production of structured nanoceramics, cutting tools for industrial applications, filters for industry
and the functional nanoceramics like optical elements or biomedical implants.
Keywords: Nanoceramics, nanopowder, sintering, compaction.
1 Introduction
The nanostructured materials are definitely not new in the ceramic field, since the nature of the
minerals employed in formulating the porcelain has resulted in ‘nanoscale’ features (the dimensions
below 100 nm) [1]. The development of physical synthesis by gas condensation initiated relatively recent
research in the field of purposely nanostructured ceramics [2]. In the last decades, nanostructured
materials were found suitable in many advanced technologies such as thermomechanics, aerospace,
nuclear power plant and biomedicine [3], especially in form of nanoceramic and nanocomposite coatings
[4] or thin films [5].
Preparation of nanomaterials like nanoceramics is a complex process starting from the synthesis of
oxide nanoparticles precursors and ending with the sintering [6]. The process involves several major
steps: a powder mix production with a bunch of powder and plasticizers for molding material, the
formation of the workpiece, drying and calcining the preform, treating the obtained product (mechanical,
thermal treatment and metallization). In some applications, the pulsed electrical current was found
useful in two-step sintering process of transparent Al
2
O
3
ceramics [7]. The properties of the resulting
material to a large extent depend on the characteristics of the nanopowders used, foremost among which
are the particle size, polydispersity and purity (contaminations content) [8].
One of the priorities for creating of new nanomaterials with specific functional properties is to search
for a fundamentally new and improvement of existing technological solutions in the field of chemical
synthesis of nanopowders and their subsequent consolidation in the solid substance. The paper is focused
on the effective synthesis and consolidation technologies that may be applied for the sintering of the
nanoceramics of various functional properties.
2 Synthesis of Nanopowders
Among a wide range of industrial and biomedical applications [9], nanoceramics developed by the
authors of this project are suitable for the following ones:
1. Structural nanoceramics:
Journal of Advances in Nanomaterials, Vol. 2, No. 3, September 2017
https://dx.doi.org/10.22606/jan.2017.23003 153
Copyright © 2017 Isaac Scientific Publishing JAN