Research Article
Glutaraldehyde-PolymerizedHemoglobin:InSearchofImproved
PerformanceasOxygenCarrierinHemorrhageModels
AncaD.Farcas,
1,2,3
VladAlToma,
1,2,3
IoanaRoman,
1
BogdanSevastre,
4
FlorinaScurtu,
2
andRaduSilaghi-Dumitrescu
2
1
Institute of Biological Research Cluj, Cluj-Napoca 400113, Branch of NIRDBS Bucharest, Romania
2
Department of Chemistry and Chemical Engineering, Babes ¸-Bolyai University, Cluj-Napoca 400028, Romania
3
National Institute for Research and Development of Isotopic and Molecular Technologies, 400293 Cluj-Napoca, Romania
4
Department of Pathophysiology, University of Agricultural Sciences and Veterinary Medicine, Cluj-Napoca 400372, Romania
Correspondence should be addressed to Radu Silaghi-Dumitrescu; rsilaghi@chem.ubbcluj.ro
Received 6 December 2019; Revised 29 March 2020; Accepted 5 August 2020; Published 1 September 2020
Academic Editor: Guillermo Mendoza-Diaz
Copyright©2020AncaD.Farcasetal.isisanopenaccessarticledistributedundertheCreativeCommonsAttributionLicense,
which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Hemoglobin- (Hb-) based oxygen carriers (HBOC) have for several decades been explored for treatment of hemorrhage. In our
previous top-up tests, HBOC with lower in vitro prooxidant reactivity (incorporating a peroxidase or serum albumin to this end)
showed a measurable but small improvement of oxidative stress-related parameters. Here, such HBOCs are tested in a hem-
orrhage set-up; ovine hemoglobin is also tested for the first time in such a setting, based on in vitro data showing its improved
performance versus bovine Hb against oxidative and nitrosative stress agents. Indeed, ovine Hb performs better than bovine Hb in
terms of survival rates, arterial tension, immunology, and histology. On the other hand, unlike in the top-up models, where the
nonheme peroxidase rubrerythrin as well as bovine serum albumin copolymerized with Hb were shown to improve the per-
formance of HBOC, in the present hemorrhage models rubrerythrin fails dramatically as HBOC ingredient (with a distinct
immunological reaction), whereas serum albumin appears not feasible if its source is a different species (i.e., bovine serum
albumin fares distinctly worse than rat serum albumin, in HBOC transfusions in rats). An effect of the matrix in which the HBOCs
are dissolved (PBS versus gelofusine versus plasma) is noted.
1.Introduction
Hemoglobin-based oxygen carriers (HBOCs) have for sev-
eral decades been proposed and tested for treatment of
hemorrhage. For preparation of these, polymerization with
glutaraldehyde has been one of the most often employed
techniques; in fact, bovine hemoglobin polymerized with
glutaraldehyde is currently approved for limited human use
in two countries, while no other HBOC is to our knowledge
currently approved for clinical use anywhere else [1–12].
Attempts to improve over the hemoglobin-glutaraldehyde
polymer have been extensively reported, including copoly-
merization with antioxidant components (albumin, heme
and nonheme peroxidases, superoxide dismutases, and small
antioxidants) or with other proteins meant to interact with
blood components (fibrinogen and carbonic anhydrase),
encapsulation, and modulation of the matrix/solution in
which the HBOC is dissolved [1, 2, 9, 10, 12–21]. Other
approaches, not involving glutaraldehyde (or involving it as
an auxiliary), have involved derivatization with inert high-
molecular weight organic polymers (e.g., polyethylene gly-
col), polymerization with other bifunctional reagents, re-
placement of bovine hemoglobin with other hemoglobins
(human, or from other organisms including plants) or even
with other proteins (hemerythrin) or even protein-free
approaches (oxygen-encapsulating emulsions, fluorinated
hydrocarbons, and heme-based dendrimers) [8, 20, 22–24].
We have previously reported an evaluation of a range of
physiological parameters in rats injected with small amounts
of blood substitute candidates based on hemoglobin [25].
ese candidates were mostly nanosized polycondensates/
polymers, as shown by chromatographic and spectroscopic
Hindawi
Bioinorganic Chemistry and Applications
Volume 2020, Article ID 1096573, 11 pages
https://doi.org/10.1155/2020/1096573