International Journal of Pure & Applied Chemistry
Vol. 6 • No. 3 • July-September 2011
pp. 353-356
I J P A C
© Global Research Publications
* To whom correspondence be made:
E-mail: reyhanbagdat@yahoo.com
Thin Layer Chromatography (TLC) Separation of Some
Medicinal and Aromatic Plants
Reyhan Bahtıyarca Bagdat
Central Research Institute for Field Crops P Box: 24 0670 Yenimahalle/Ankara
ABSTRACT: TLC (Thin layer chromatography) separation of sage (Salvia officinalis), lemonbalm (Melissa
officinalis), thyme (Thymus vulgaris) and mountain tea (Sideritis perfoliata) was performed in this research.
Essential oils and extracts of these drugs were loaded in various quantities to Kiesegel 60 glass plates using
several solvents and different doses separately. Plant extracts were condensed under Nitrogen gas flow (3:1).
Five different dyeing methods were used after achieving the reference plate. Guaiazulene (8 µl) and Liphophilic
(10 µl) were used as references in every treatment. Their lay outs were investigated under visual and 254-366
nm UV light. Toluol:Ethylacetate (93:7) as solvent and Anisaldehyde-H
2
SO
4
as dyeing material gave good
separation and result.
Keywords: TLC Separation, sage (Salvia officinalis), lemon balm (Melissa officinalis), thyme (Thymus vulgaris),
mountain tea (Sideritis perfoliata)
INTRODUCTION
Turkey has the largest flora of any European
or Mediterranean country and as a consequence
the largest number of medicinal plants
species in the Europe and Middle East.
Approximately 28,000 tonnes of medicinal
and aromatic plants are exported annually,
generating nearly 50 million dollars of foreign
currency from the trade. This trade has helped to
earn 20 times more income compared to one
earned through bulbous plants marketed for
horticultural purpose. Lange & Schippmann,
(1997) and Anonymous (2003) indicate that Turkey
is the third largest exporter of medicinal plants of
wild origin of any country on earth after China
and India.
Sage (Salvia officinalis), lemon balm (Melissa
officinalis), thyme ( Thymus vulgaris) are well
known medicinal and aromatic plants widely used
in folk medicines. Mountain tea ( Sideritis
perfoliata) is, consumed commonly as herbal tea
in Aegean and Mediterennean coastal regions of
Turkey. The traditional medicinal plants are
mostly used for the treatment of wounds (25.3%),
cold and influenza (24.6%), stomach disorders
(20%), cough (19%), kidney ailments (18.2%) and
diabetes (13.4%) (Kultur, 2006).
TLC (thin layer chromatography) is a simple,
quick, and inexpensive procedure that gives a
quick answer as to how many components are in
a mixture. It can be also used to support the
identity of a compound in a mixture when the R
f
of a compound is compared with the R
f
of a known
compound (preferably both run on the same TLC
plate). Once visible, the R
f
value (Retention factor),
of each spot can be determined by dividing the
distance traveled by the product by the total
distance traveled by the solvent (the solvent front).
These values depend on the solvent used, and the
type of TLC plate, and are not physical constants
(Harwood et al. 1999; Reich and Schibli, 2007).
TLC may be a useful method in medicinal and
aromatic plant breeding to make a quick
comparison or selection between or among the
components of different promising lines to develop
new cultivars.
MATERIAL AND METHODS
Extracts and essential oils from sage ( Salvia
officinalis), thyme (Thymus vulgaris), lemon balm
(Melissa officinalis) and mountain tea (Sideritis
perfoliata) were used as material with the applied