1429 © 2012 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim wileyonlinelibrary.com small 2012, 8, No. 9, 1429–1435
1. Introduction
Graphene is a promising material for electronics due to its
unique transport properties such as high carrier mobility,
[1,2]
quantum Hall effect at room temperature,
[3,4]
ballistic trans-
port,
[5–7]
and so on. Many studies focused on the methods
to obtain graphene. Micromechanically cleaved graphene on
silicon dioxide substrate
[8,9]
is widely used for fundamental
research but is less useful for scaled-up applications due to
its low yield. Epitaxial growth on silicon carbide (SiC)
[10–12]
and chemical vapor deposition (CVD) on catalytic metal
surfaces by surface precipitation
[13,14]
or dissociation
[15–17]
allow scaled-up production of graphene, but these growth
approaches are usually carried out at rather high tempera-
tures and transfer techniques are usually required when
Growth, Characterization, and Properties of
Nanographene
Wei Yang, Congli He, Lianchang Zhang, Yi Wang, Zhiwen Shi, Meng Cheng,
Guibai Xie, Duoming Wang, Rong Yang, Dongxia Shi, and Guangyu Zhang*
applying such materials on a nonspecific substrate. To avoid
transfer or post-treatment processes, many approaches
were developed. For example, Ismach et al. grew graphene
on a sacrificial Cu layer
[18]
which can be evaporated away
during synthesis; however, the evaporation of metal films
still requires a high-temperature process. Rummeli et al.
reported a low-temperature synthesis of nanographene via
CVD,
[19]
but the growth succeeded only on magnesium oxide
(MgO). In 2011, we reported the low-temperature (~550 °C)
and catalyst-free growth of nanographene films on various
substrates by using a remote plasma-enhanced chemical
vapor deposition (RPECVD) system.
[20]
This new growth
technique for nanographene is low-cost and compatible
with existing semiconductor processing technologies. These
nanographene films are optically transparent, mechanically
flexible, and electrically conductive with tunable charge-car-
rier densities, which indicates great potential in the field of
thin-film resistors, electrode materials, and transparent con-
ductive films. Moreover, nanographene films have abundant
edges, which can be easily functionalized by various chem-
ical groups, and thus they are useful for various catalysts or
chemical sensors.
Here we present a systematic study of nanographene films
with focus on their electrical transport properties. Firstly, we
review the growth of nanographene films, followed by their DOI: 10.1002/smll.201101827
W. Yang, C. L. He, L. C. Zhang, Y. Wang, Z. W. Shi,
M. Cheng, G. B. Xie, D. M. Wang, R. Yang,
Prof. D. X. Shi, Prof. G. Y. Zhang
Beijing National Laboratory for Condensed Matter
Physics and Institute of Physics
Chinese Academy of Sciences
Beijing 100190, P. R. China
E-mail: gyzhang@aphy.iphy.ac.cn
A systematic study on nanographene grown directly on silicon dioxide substrates
is reported. The growth is carried out in a remote plasma-enhanced chemical vapor
deposition system at a low temperature of around 550 °C with methane gas as the
carbon source. Atomic force microscopy is used to characterize the nanographene
morphology, and Raman spectroscopy, X-ray photoelectron spectroscopy, and
scanning tunneling microscopy are exploited to identify the in-plane sp
2
bonding
structures of nanographene samples. Electrical transport properties are measured
at various temperatures down to 4 K. Tunneling effects, minimal conductance at the
charge-neutral point, sheet resistances, and Dirac point position at different channel
lengths are investigated. In addition, nanographene film possesses high transmittance
properties, as indicated by transmittance spectra. Nanographene devices are fabricated
from rippled structures, and show great promise for strain-gauge sensor applications.
Nanographene