A publication of
CHEMICAL ENGINEERING TRANSACTIONS
VOL. 34, 2013
The Italian Association
of Chemical Engineering
Online at: www.aidic.it/cet
Guest Editors: Neven Duić, Petar Sabev Varbanov
Copyright © 2013, AIDIC Servizi S.r.l.,
I SBN 978-88-95608-25-9; I SSN 1974-9791 DOI: 10.3303/CET1334004
Please cite this article as: Andoni A., van Santen R. A., 2013, Propenal hydrogenation on silver surface-a theoretical
approach, Chemical Engineering Transactions, 34, 19-24 DOI:10.3303/CET1334004
19
Propenal Hydrogenation on Silver Surface -
A Theoretical Approach
Adelaida Andoni*
,a
, Rutger A. van Santen
b
a
Department of Chemistry, Faculty of Natural Sciences, University of Tirana, Blv. “Zog I”, 1001, Tirana, Albania
b
Department of Inorganic Chemistry and Catalysis, Schuit Institute of Catalysis, Eindhoven University of Technology,
P.O. Box 513, 5600 MB, Eindhoven, The Netherlands
adelaida.andoni@unitir.edu.al
Catalytic reactions perform best if the interaction between the adsorbates and the surface is not too strong
and not too weak. This relates to the d-band occupancy of the metals. In this respect, hydrogenation of
propenal or acrolein on silver surface rises up the question whether H
2
proceeds in the mechanism of the
reaction as molecule or dissociates on silver. Silver having an electronic configuration 4d
10
5s
1
cannot
dissociate the strong bond of H
2
. However, it is known that even on gold provided the gold particles are
very small molecules such as O
2
can dissociatively chemisorb. Aiming elucidation of the reaction
mechanism, small clusters of silver atoms are considered (mimicking small particles) by checking first their
stability by means of theoretical calculations. Next, adsorption of hydrogen was allowed in order to
estimate whether the adsorption energy is exothermic or not. In this context, computational calculations
carried out by means of Density Functional Theory for small silver clusters indicated that rhombic structure
was the most stable configuration. Adsorption of hydrogen on rhombic silver cluster yielded negative value
of the adsorption energy suggesting that hydrogen can dissociatively be adsorbed on small particle and
step surfaces as well.
1. Introduction
Catalysts may make significant difference in reaction rate. For example, a hydrogen/oxygen mixture may
be stable for years at 25 °C. Nevertheless, if one introduces a platinum wire into the mixture, the mixture
explodes. Another introductory example is the key reaction in the cleaning automotive exhaust, the
catalytic oxidation of CO to CO
2
on the surface of noble metals such as Pt, Pd, Rh and Au-Cu (Liu et al.
2011) as well as over FeOx-supported Pd catalyst (Liu et al. 2012). Reduction of CO
2
, on the other hand,
remains challenging as recently reported (Siitonen and Ahtila, 2009). Selective catalytic hydrogenation of
organic α-β unsaturated aldehydes (for example, propenal or acrolein) is a reaction with important
applications in the industrial field (Bron et al. 2007). It gives the following types of products (Figure 1).
The most important product from an industrial point of view is the unsaturated alcohol, which is also the
most difficult to obtain since it is known that the hydrogenation of the C=C group in α-β unsaturated
aldehydes is more favourable than the hydrogenation of C=O group (Bron et al. 2007). To improve the
selectivity towards the unsaturated alcohol several attempts are made to develop a catalytic system
suitable for this reaction (Bron et al. 2007). It is known that monometallic silver is able to hydrogenate
selectively the C=O group of α-β unsaturated aldehydes in the gas phase (silver having a low value of the
heat of adsorption for hydrogen can preferentially hydrogenate the C=O group because strongly adsorbed
hydrogen reacts more readily with the C=C group than weakly adsorbed hydrogen). It is assumed that the
first step of the reaction is the dissociation of hydrogen on silver and the second one is the hydrogenation
of double bonds C=C and C=O (Bron et al. 2007). Nevertheless from catalysis point of view, as we go from
the left to the right in a row of the periodic table the tendency in the reactivity of metals changes as shown
in Figure 2 (Chokendorf and Niemantsverdriet, 2003).