Research Journal of Agriculture and Environmental Management. Vol. 3(10), pp. 511-518, October, 2014
Available online at http://www.apexjournal.org
ISSN 2315 - 8719© 2014 Apex Journal International
Full Length Research
Study of hydro-distillation process of Ruta chalepensis
L. essential oil
Jamel Mejri
1,2 *
, Iheb Chakroun
3
, Manef Abderrabba
1
, and Mondher Mejri
1
1
Laboratoire Matériaux Molécules et Applications, Institut Préparatoire des Etudes Scientifiques et Techniques, IPEST,
BP51, La Marsa 2070, Tunisia.
2
Département Génie Mécanique et Agro-Industriel, Ecole Supérieure des Ingénieurs de l’Equipement Rural, ESIER,
9070 Medjez el Bab, Tunisia.
3
Ecole Supérieure des Industries Alimentaires de Tunis, Cité El Khadhra Tunis – 1003, Tunisia.
Accepted 15 September, 2014
The hydrodistillation of essential oil from aerial part of Ruta chalepensis L. (rue oil) was studied. Two
models were applied: first order kinetic model and Monod model. Models were evaluated to predict the
recovered essential oil. Process parameters optimization for hydrodistillation was reported. The
hydrodistillation did not follow very well the first order kinetic model. Monod model kinetic was shown
to simulate hydrodistillation rue oil. The highest oil yield was obtained during the period extending from
March to April with a hydrodistillation duration superior to 100 minutes. It was observed that yield can
be modeled as function of growth stage. GC-MS analysis showed that the major constituent of the oil
was 2-undecanone (77.7%).
Key words: Ruta chalepensis L., Essential oil, Hydrodistillation, Kinetic, Monod model, Simulation.
INTRODUCTION
Essential oils have extensively been studied because of
their commercial interest (Da Porto et al., 2009). They
have been employed in the fragrance industry, in
aromatherapy, in pharmaceutical preparations and in
food manufacturing as functional ingredients (Rezzoug et
al., 2005; Magwa et al., 2005; Tepe et al., 2005; Chemat
et al., 2006; Cassel et al., 2009). The development of
essential oil sector has a direct relation with the
improvement of process technology in industrial plants
(Cassel et al., 2009). Hydrodistillation is normally used to
isolate essential oils from aromatic and medicinal plants
(Velickovic et al., 2008).
A common characteristic of the processes of extraction
and purification of natural products is the need to know
the system, which allows the definition of the process
operation conditions (Teixeira de Souza et al., 2008). For
a possible industrial application, the optimization and the
*Corresponding author. E-mail: jmejri2001@yahoo.fr Tel: +216
97 577 532; Fax: + 216 78 561 700
assessment of the extraction process with mathematical
modeling seem to be essential (Liu et al., 2009). This
experimental methodology combines mathematics with
statistics for generating a mathematical model to describe
the process, analyzing the effects of the independent
variables and optimizing the processing operations (Liu et
al., 2009).
Different mathematical models were used to simulate
hydrodistillation and steam distillation of essential oil.
Such models were used to generalize the experimental
results. Benyoussef et al. (2002) showed that the kinetic
model simulates very well essential oil hydrodistillation
from coriander seeds than diffusional model. Hanci et al.
(2003) proposed a logarithmic model. Koul et al. (2004)
shows that extraction of oil by steam distillation of grass
follows first order kinetics. However, Babu and Singh
(2009) demonstrated that the oil produced by
hydrodistillation from E. cinerea did not follow the first
order kinetic model, but the process can be simulated by
Langmuir gas adsorption model. Works of Cassel et al.
(2009) indicated that diffusional model fitted very well the
experimental data for the essential oil recovered by