TASTE ABATEMENT AND CHARACTERIZATION OF DISPERSIBLE TABLETS OF ARTEMETHER
PREPARED BY HOT MELT EXTRUSION
Original Article
YOGESH A. SONAR
1*
, MRUDULA H. BELE
2
, NITIN H. SONAR
3
, VISHAL S. BAGUL
4
, PRASHIK S. SHIMPI
5
1,2
Pharmaceutics Department of NDMVP Samaj’s College of Pharmacy, Nashik, 422002,
3,4,5
Received: 02 May 2017, Revised and Accepted: 10 Oct 2017
R C Patel Institute of Pharmaceutical Education
and Research, Shirpur, 425405
Email: yshsonar@gmail.com
ABSTRACT
Objective: The aim of this study was to formulate and evaluate a taste-masked formulation using hot melt extrusion approach for artemether.
Methods: Taste masking of artemether was done by preparing solid dispersion with coating polymer kollicoatsmartseal 30D using hot melt extrusion. The
prepared solid dispersion was subjected to taste masking evaluation like sensory evaluation parameters against five levels set for taste evaluation using
artemether as control standard along with in vitro release studies in simulated salivery fluid. After taste evaluation of solid dispersion was subjected to the
formulation of dispersible tablets by direct compression method. The final taste masking evaluation of dispersible tablets of solid dispersion containing
artemether were done by a sensory evaluation panel of nine members along with in vitro release study in simulated salivary and gastric fluid.
Results: The percent drug content was found 35.09±0.06 % in solid dispersion. The drug excipients compatibility studies performed with the help
of FTIR instrument and DSC that indicates there were no interactions between drug and polymers. Solid dispersions (1:1, 1:2, 1:3 drug polymer
ratio) of artemether were evaluated by sensory evaluation panel from which 1:3 drug: polymer solid dispersion was found more palatable. Release
rate study in simulated salivary fluid shown no release but shows release of drug in simulated gastric fluids which indicates that the drug was taste
masked. The optimized batch of dispersible tablets (F1) were subjected for evaluation parameters like dispersion time (70±1.90), wetting time
(63±1.86), etc. Dissolution studies of optimized formulation indicated that the polymer does not allow drug to release in simulated salivery pH 6.8
but shows immediate release in simulated gastric pH which also confirms taste masking efficiency of polymer. Final optimized F1 batch evaluated
for taste masking evaluation by sensory evaluation panel using pure drug as control standard found to be palatable.
Conclusion: It may be concluded that kollicoatsmartseal 30D could mask the taste of the drug in salivary pH and shows drug release at gastric pH
which confirms its efficiency for taste masking.
Keywords: Artemether, Kollicoatsmartseal 30D, Hot-melt extrusion, Taste masking, Solid dispersion
© 2017 The Authors. Published by Innovare Academic Sciences Pvt Ltd. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/)
DOI: http://dx.doi.org/10.22159/ijap.2017v9i6.19555
INTRODUCTION
Worst the taste of the medication, the better the cure was once the
prevailing attitude. Today this trend has changed and great
importance is placed on the organoleptic characteristics of
pharmaceutical products [1]. Oral administration of pharmaceuticals
is one of the most popular method of drug delivery [2]. Organoleptic
characteristics of pharmaceutical products, i.e. Taste, odor, and
appearance are essential factors in assessing the patient acceptability;
out of these organoleptic characteristics of taste is an important
parameter governing patient compliance [3]. Some active
pharmaceutical ingredients (API's) are generally associated with an
unpleasant taste. The formulations containing such APIs are poorly
accepted by patients and the adherence to treatment is adversely
affected. Bad taste is a primary barrier while administering drugs to
children. Most of the pediatricians reported that the taste and
palatability were the greatest hurdles to complete treatment.
Therefore. It is necessary to discover robust approaches to formulate
the dosage forms to mask the unpleasant taste of the API to improve
the ease of administration and palatability. Oral administration of
bitter drugs with an acceptable degree of palatability is a key issue for
health care providers, especially for pediatric patients. Taste masking
in the present day pharmaceutical industry has become a potential
tool to improve patient compliance and commercial success of the
product [3-6]. The taste of any substance can be improved by two
basic manipulations; either by reducing the drug solubility or by
altering the ability of the drug to interact with taste receptors [7].
Artemether (ARM) drug used for the prevention of malaria and is
included in the WHO list of essential medicines. Artemether is
essential for rapid clearance of parasitemia and rapid resolution of
symptoms. It reduces parasite numbers by a factor of approximately
10,000 in each asexual cycle, which is more than other current
antimalarial (which reduce parasite numbers 100–1000-fold per
cycle). Artemether is active against P. vivax as well as chloroquine
sensitive and chloroquine resistant strains of P. falciparum and is
also indicated in the treatment of cerebral malaria [8-12].
The objective of this study was to developed taste masked formulation of
artemether which is intensely bitter in taste and is a critical problem,
especially in the pediatric population. Hence, to increase the palatability
of the drug it is necessary to mask the taste and to formulate a suitable
dosage form to enhance patient compliance and adherence to treatment.
On this background, this research was designed to address the question,
whether it is possible to mask the intensely bitter taste of the poorly
water soluble drug ‘Artemether’ by hot melt extrusionusing the
kollicoatsmartseal 30D as a polymer for taste abatement?
Oro-dispersible tablets (ODTs) entered the market in the 1980s as
an alternative to tablets and it also provides an advantage
particularly for pediatric and geriatric populations who have
difficulty in swallowing conventional tablets and capsules
MATERIALS AND METHODS
[13].
Materials
Artemether was received as a gift sample from ajanta pharma
limited. aurangabad and IPCA laboratories limited. ratlam, India.
kollicoatsmartseal 30 D was received as a gift sample from the BASF
chemical company, mumbai, India. Potassium dihydrogen phosphate
procured from modern Scientifics, nashik-India. Materials were used
as received.
Methods
Preparation of drug: polymer solid dispersion by hot melt
extrusion (HME)
The HME was optimized by trial and error method with the help of
data obtained from previous work. It was optimized first using
International Journal of Applied Pharmaceutics
ISSN- 0975-7058 Vol 9, Issue 6, 2017