1
Supporting Information
Rec. Nat. Prod. 11:6 (2017) 552-557
Chemical and Biological Investigation of Ochrosia elliptica Labill.
Cultivated in Egypt
Riham A. El-shiekh
1
, Dalia A. Al-Mahdy
1
, Mohamed S. Hifnawy
1
,
Tzvetomira Tzanova
2
, Emilie Evain-Bana
2
, Stéphanie Philippot
2
,
Denyse Bagrel
2
, Essam A. Abdelsattar
1,
*
1
Department of Pharmacognosy, Faculty of Pharmacy, Cairo University, Kasr El Aini st.,
P.B. 11562, Egypt,
2
Molecular Engineering Laboratory and Pharmacological Biochemistry (LIMBP), Jean
Barriol Institute, University of Lorraine, Metz, France
Table of Contents Page
1 Experimental 3
1.1 Plant materials
1.2 General Experimental Procedures
1.3 Chemicals and Reagents
3
3
3
1.4 Extraction and Isolation 3
1.5 Biological Evaluation 3
1.5.1 Cell lines and culture conditions 3
1.5.2 Cell viability determination (MTT assay) 3
1.5.3 Evaluation of CDC25s inhibitory potential 3
1.5.4 In-vitro antioxidant activity 4
1.5.5 Determination of the median lethal dose (LD50) 4
1.5.6 In-vivo anti-inflammatory activity 4
1.5.7 Statistical analysis 5
2 Spectroscopic data and characterization 5
S1:
1
H-NMR (400 MHz, CDCl
3
) spectrum of Lupeol acetate (1) 6
S2:
13
C-NMR (100 MHz, CDCl
3
) spectrum of Lupeol acetate (1) 7
S3: ESI-MS spectrum of Lupeol (2) 8
S4:
1
H-NMR (400 MHz, CDCl
3
) spectrum of Lupeol (2) 9