ORIGINAL ARTICLE
A fed-batch based cultivation mode in Escherichia coli
results in improved specific activity of a novel chimeric
-truncated form of tissue plasminogen activator
F. Mahboudi, F. Barkhordari, R.M. Godarzi, S. Enayati and F. Davami
Biotechnology Research Center, Pasteur Institute of Iran, Tehran, Iran
Keywords
Escherichia coli expression, fed-batch
cultivation, specific activity, tissue-type
plasminogen activator.
Correspondence
Fatemeh Davami, Biotechnology Research
Center, Pasteur Institute of Iran (IPI), No.
358, 12th Farvardin Ave, Jomhhoori St,
Tehran 1316943551, Iran. E-mail:
f_davami@pasteur.ac.ir
2013/1633: received 12 September 2012,
revised 29 October 2012 and accepted 29
October 2012
doi:10.1111/jam.12059
Abstract
Aims: A novel chimeric-truncated form of tissue-type plasminogen activator
(t-PA) with improved fibrin affinity and resistance to PAI was successfully
produced in CHO expression system during our previous studies. Considering
advantages of prokaryotic expression systems, the aim in this study was to
produce the novel protein in Escherichia coli (BL21) strain and compare the
protein potency in batch and fed-batch processes.
Methods and Results: The expression cassette for the novel t-PA was prepared
in pET-28a(+). The E. coli expression procedure was compared in traditional
batch and newly developed fed batch, EnBase
®
Flo system. The protein was
purified in soluble format, and potency results were identified using
Chromolize t-PA Assay Kit. The fed-batch fermentation mode, coupled with a
Ni-NTA affinity purification procedure under native condition, resulted in
higher amounts of soluble protein, and about a 30% of improvement in the
specific activity of the resulted recombinant protein (46Á66 IU mg
À1
)
compared to traditional batch mode (35Á8 IU mg
À1
).
Conclusions: Considering the undeniable advantages of expression in the
prokaryotic expression systems such as E. coli for recombinant protein
production, applying alternative methods of cultivation is a promising
approach. In this study, fed-batch cultivation methods showed the potential to
replace miss-folded formats of protein with proper folded, soluble form with
improved potency.
Significance and Impact of the Study: Escherichia coli expression of recombinant
proteins still counts for nearly 40% of marketed biopharmaceuticals. The major
drawback of this system is the lack of appropriate post-translational
modifications, which may cause potency loss/decline. Therefore, applying
alternative methods of cultivation as investigated here is a promising approach to
overcome potency decrease problem in this protein production system.
Introduction
Tissue-type plasminogen activator (t-PA) is a glycopro-
tein consisting of 527 amino acid residues (72 kDa),
which is FDA approved for the treatment of myocardial
infarction. Enhanced activity in the presence of fibrin,
that is, fibrin-specific plasminogen activation, is the
major advantage of t-PA over other thrombolytic agents.
Bowes melanoma cells were the first source of t-PA as
a therapeutic (Griffiths and Electricwala 1987). To meet
the need for sufficient production of the drug through a
robust industrial process, recombinant t-PA (rt-PA) was
produced in mammalian cells (Lubiniecki et al. 1990;
Cartwright 1992). However, low volumetric yields of the
recombinant protein, long cultivation times and the need
for expensive bioreactors and medium components are
364 Journal of Applied Microbiology 114, 364--372 © 2012 The Society for Applied Microbiology
Journal of Applied Microbiology ISSN 1364-5072