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Department of Physics, Jadavpur University, Jadavpur, Kolkata700 032, India
Department of Physics, Behala College, Kolkata700 060, India
( Crystallographic data and refinement parameters of complex (
Crystal data
Formula C
7
H
9
CoNO
7
Formula Weight 278.08
Crystal System Orthorhombic
Space group P2
1
2
1
2
1
(No. 19)
a [Å] 9.3953(1)
b [Å] 7.3422(1)
c [Å] 13.9495(2)
V [Å
3
] 962.27(2)
Z 4
D(calc) [g/cm
3
] 1.919
;(MoKα)[mm] 1.805
F(000) 564
Crystal Size [mm] 0.15 x 0.17 x 0.20
Temperature (K) 295
Radiation [Å] MoKα 0.71073
Θ MinMax [°] 2.6, 25.3
Dataset 11: 11 ; 8: 8 ; 16: 16
Total 7279
Unique Data 1753
R(int) 0.034
Observed[I > 2.0 σ(I)] 1694
Nref 1753
Npar 145
R 0.0281
wR2 0.0746
S 1.11
Max. and Av. σ/esd 0.00, 0.00
Min. and Max. ∆ρ [e/Å
3
] 0.46, 0.41
w = 1/[\s^2^(Fo^2^)+(0.0410P)^2^+0.5333P] where P=(Fo^2^+2Fc^2^)/3