Vol.:(0123456789) 1 3
Journal of Sedimentary Environments (2021) 6:1–12
https://doi.org/10.1007/s43217-020-00040-5
ORIGINAL ARTICLE
Rare‑earth element (REE) geochemistry of late Paleocene–middle
Eocene phosphate nodules in the Subathu Basin of Solan District,
Himachal Pradesh, India
M. Shuaib
1
· K. F. Khan
1
· A. Hussain
1
· M. Jawad
1
· Shamim A. Dar
2
Received: 27 August 2020 / Revised: 21 November 2020 / Accepted: 2 December 2020 / Published online: 4 January 2021
© The Author(s), under exclusive licence to Springer Nature Switzerland AG part of Springer Nature 2021
Abstract
The phosphate nodules are solely confned to the Green facies of late Paleocene–middle Eocene Subathu Formation in the
Subathu Basin of Solan District, Himachal Pradesh, India. The phosphate nodules are hard and compact, elliptical, rounded
to well rounded, usually dull earthy to dark grayish in color and break with sharp and conchoidal surfaces. The present study
deals with the rare-earth elements (REE) geochemical characteristics viz. hat-shaped, enrichment of middle REE relative to
light REE and heavy REE, negative Eu and weak negative to weak positive Ce anomalies and values of ratios such as Er/Nd
(0.07–0.19), Y/Ho (32–48), La/Nd (0.46–0.90), (La/Sm)
N
(0.18–0.47) and (La/Yb)
N
(0.26–0.51). It appears that the seawater
conditions or growth mechanisms were diferent at the time of formation of cores and rims of the nodules as indicated by
the contrast REE concentrations, respectively. Although in both cases very similar REE spectra are observed, rims are much
more likely to show a diagenetic alteration front than cores. The Y/Ho ratio (32–48) suggests that the principal source of
REE was the terrigenous sediments followed by seawater in the rims and cores of these nodules. The results of this study
suggest a dominant role of diagenetic processes in the REE concentration and distribution as well as possible suboxic to
anoxic conditions during the formation of cores and rims of phosphate nodules, as also evident by the presence of pyritic
nodules in the Subathu Basin of Solan District.
Keywords REE geochemistry · Phosphate nodules · Solan · Subathu formation · Middle REE · Diagenetic processes
1 Introduction
Marine sediments are known to host phosphate nodules
throughout the geological past (Stalder and Rozendaal
2004) and in recent sediments of phosphatic nature (Ras-
mussen et al. 1998; Jiang et al. 2007). Phosphate sediments
in diatomaceous organic-rich layers have been reported at
the western margin of South Africa, continental margin of
Peru–Chile and Baja California of Mexico (Veeh et al. 1973;
Birch 1979; Schufert et al. 1994). These are areas of ocean
high productivity zones of organic matter in the world. How-
ever, according to O’Brien et al. (1981), low productivity
zones of oceans also show the presence of phosphates where
assimilation of phosphorus was probably attributed by the
presence of organic matter and bacteria.
It is well known that signifcant concentration of REE can
be incorporated in phosphate nodules at the time of early
diagenesis during their growth in marine sediments (Kidder
et al. 2003). The REE geochemistry of phosphorites can be
used as a tool to characterize a depositional environment
because various REE profles are seen in diferent marine
depositional conditions. For example, cerium depletions
refect exposure to oxidized seawater, fat patterns are inter-
preted to display detrital infuence, and light REE depletions
suggest the infuence of weathering. In phosphatic sedi-
ments, the original seawater REE pattern and its concentra-
tions may be altered by various processes such as weather-
ing, burial diagenesis, and metamorphism (McArthur and
Walsh 1984; Fazio et al. 2007), so, the REE concentration
and its distribution in phosphates can vary from one basin
Communicated by M. V. Alves Martins
* M. Shuaib
shuaibamu16@gmail.com
1
Department of Geology, Aligarh Muslim University,
Aligarh 202002, UP, India
2
Department of Geology, Centre of Advanced Study, Institute
of Science, Banaras Hindu University, Varanasi 221005,
India