Original Article
MICROBIAL SYNTHESIS OF SILVER NANOPARTICLES USING STREPTOMYCES SP. PG12 AND
THEIR CHARACTERIZATION, ANTIMICROBIAL ACTIVITY AND CYTOTOXICITY ASSESSMENT
AGAINST HUMAN LUNG (A549) AND BREAST (MCF-7) CANCER CELL LINES
PALLAVI S. S.
a
, MEGHASHYAMA PRABHAKARA BHAT
a
, SREENIVASA NAYAKA
a*
a
P. G. Department of Studies in Botany, Karnatak University, Dharwad 580003, Karnataka, India
Email: sreenivasankud@gmail.com
Received: 23 Apr 2021, Revised and Accepted: 22 Jun 2021
ABSTRACT
Objective: Synthesis of silver nanoparticles using Streptomyces sp. PG12 and their characterization, antimicrobial activity and cytotoxicity against
A549 and MCF-7 cancer cell lines.
Methods: The silver nanoparticles were subjected to UV-Vis. spectroscopy, Fourier transform infrared spectroscopy (FTIR), scanning electron
microscopy with energy-dispersive X-ray spectroscopy (SEM/EDS), high-resolution transmission electron microscopy (HR-TEM), zeta potential,
and X-ray diffractometry (XRD) analyses. Further, the antimicrobial potential was determined by using the agar well diffusion method and
cytotoxicity was determined with the help of cell viability (MTT) assay and reactive oxygen species (ROS) assay.
Results: The initial indication of silver nanoparticles synthesis was noticed by the colour change in the reaction mixture and the absorption
maximum at 421 nm in UV-Vis. analysis; whereas, the FTIR analysis displayed the biological functional groups responsible for the capping and
stabilization of silver nanoparticles. SEM and TEM micrographs revealed the surface morphology, spherical shape, and smallest particle size as
18.91 nm. The EDS and XRD patterns confirmed the involvement of various elements during the synthesis of silver nanoparticles and the crystalline,
face-centered cubic nature, respectively. The silver nanoparticles displayed considerable antimicrobial activity against human pathogens even at
low MIC and MBC concentrations and exhibited increased anticancer activity against A549 and MCF-7 cell lines, where the ability of silver
nanoparticles to significantly restrict the growth of tumour cells was observed at IC50 values of 69.04µg/ml and 138.30µg/ml, respectively.
Conclusion: Streptomyces sp. PG12 synthesized silver nanoparticles show significant anticancer activity against A549 and MCF-7 cell lines.
Keywords: Silver nanoparticles, Streptomyces sp., Antimicrobial activity, ROS expression, Human lung and breast cancer cell lines
© 2021 The Authors. Published by Innovare Academic Sciences Pvt Ltd. This is an open access article under the CC BY license (https://creativecommons.org/licenses/by/4.0/)
DOI: https://dx.doi.org/10.22159/ijpps.2021v13i8.41876. Journal homepage: https://innovareacademics.in/journals/index.php/ijpps.
INTRODUCTION
Nanotechnology is the concept that deals with the production,
manipulation, characterization, and applications of nano-scale
materials whose size usually ranges between 1 to 100 nm. Nano-
materials prepared from metals offer unique properties of size,
shape, and larger surface area to volume ratio [1]. In the recent
decade, these metal nanoparticles prepared using gold, silver,
platinum, copper, zinc, lead, iron, and many more are extensively
used for various applications in divergent fields such as nano-
medicine, electrical, agriculture, pharmaceuticals, cosmetics, food
industry, textiles, and data storage [2, 3].
Silver is more often considered for synthesizing nanoparticles due to
potential antimicrobial, antioxidant, anti-inflammatory, and anticancer
activities. The recent advancements in nano-science have pointed out
the significance of silver nanoparticles (AgNPs) in the areas of
biomedical, DNA sequencing, biological sensors, plasmonics, catalysis,
energy generation, and clean water technology [4, 5]. Generally, AgNPs
are produced by one of two paths, i.e., ‘top-down’ or ‘bottom-up’
strategies via physical or chemical or biological synthesis routes. The
physical and chemical techniques require more energy, thermal
ablation, and hazardous chemicals that are carcinogenic and induce
genotoxicity. Hence, due to its low cost, non-toxicity, and eco-friendly
nature, the biological synthesis method is essential [6, 7].
The greener approach of AgNPs synthesis is carried out by
employing biological resources like algae, lichens, bacteria, yeast,
fungi, actinobacteria, and plant extracts. Among the microorganisms,
bacteria are considered the ideal source for metal nanoparticles
synthesis, owing to their metal resistance mechanism, which helps
them reduce ionic silver (Ag
+
) into elemental (Ag°) NPs [8, 9]. The
microbial synthesis method of AgNPs allows for safer, cheaper, and
more stable metallic AgNPs as the microbes produce various
secondary metabolites, which actively participate in the reduction,
capping, and stabilization [10].
The increasing multi-drug resistance in human pathogenic
microorganisms is of great concern, and there is an urgent need for
the development of broad-spectrum antimicrobials to treat severe
infections. The AgNPs have gained importance as the alternative for
antibacterial and antifungal agents and help reduce toxicity, avoid
the side effects in patients, and prevent pathogens [11, 12]. Cancer is
ranked top on the list of deadly diseases as the second leading cause
for the most deaths across the globe, and the numbers are expected
to increase further [13]. From the past few decades, AgNPs are
extensively used as cytotoxic agents against various human cancers.
The microbial AgNPs synthesized using species of Pseudomonas [14],
Enterococcus [15], and Streptomyces [16, 17] have successfully
prevented the growth of tumour cells.
Actinomycetes belong to Gram-positive, aerobic and filamentous
bacteria with high G+C content. Many of the Actinomycetales
members are known for their peculiar capacity to produce bioactive
secondary metabolites having properties from antimicrobial to
anticancer and many more [18-20]. Because of these essential
biological properties of actinobacterial secondary metabolites, the
culture filtrate of Streptomyces sp. PG12 was to investigate for the
extracellular synthesis of AgNPs and their evaluation for
antimicrobial and anticancer potential.
MATERIALS AND METHODS
Collection of pathogens
The pathogenic microorganisms such as Staphylococcus aureus
(MTCC6908), Pseudomonas aeruginosa (MTCC424), Enterococcus
International Journal of Pharmacy and Pharmaceutical Sciences
Print ISSN: 2656-0097 | Online ISSN: 0975-1491 Vol 13, Issue 8, 2021