Semiconductors based on heavy p‑block elements (such
as Bi, Sb, Te and Se) that crystallize in the rhombohedral
tetradymite structure have long been of interest as the
world’s best thermoelectrics (TEs) for room‑temperature
operation and have been continuously studied and
developed for that application
1
. For simplicity, we clas‑
sify them as ‘tetradymites’ after the mineral of nominal
composition, Bi
2
Te
2
S. In the past decade, tetradymites
have also emerged as important hosts for the topological
surface state, a previously unexplored electronic state of
matter.
Generally, semiconductors have surface states because
the surface represents an interruption of the periodic
potentials of the atoms in the bulk (these are Shockley
and Tamm states
2
), which creates additional energy levels
that are available to electrons at the surface. In materials
with inverted electronic band energies (BOX 1), electrons
in the surface states can be topologically protected from
back‑scattering and can develop other unusual proper‑
ties. Topological protection provides the surface state
electrons with robustness to perturbations that do not
break symmetry (time‑reversal symmetry in the case of
tetradymites). In materials called topological insulators
(TIs), electrical conduction in the bulk is expected to be
suppressed, and the topological protection of the surface
states strengthened. TIs are semiconductors in which
the constituent atoms are heavy and of similar electro‑
negativities; these materials have been reviewed exten‑
sively from the perspective of materials science
3–5
and
have also been discussed from a chemical point of view
6,7
.
It has often been stated that materials with good TE
properties are concomitantly materials with good TI
properties
8
. Tetradymites are important materials in both
of these areas of materials science (Bi
2
Se
3
has been called
‘the hydrogen atom of TIs’).
Although topological physical concepts are novel,
exciting and newsworthy, it is topological materials that
have turned these concepts into reality and enabled the
field to engage experimentalists as well as theoreticians.
Two kinds of materials initially displayed topological
properties
3–5
, the bismuth–antimony alloy semiconductor
Bi
1 − x
Sb
x
( x ≈ 5 to 20 at%) and thin‑film heterostructures of
(Hg,Cd)Te. Both of these materials have limitations that
have precluded their widespread experimental study. For
bismuth–antimony alloys, the normal surface states that
exist on the crystal surfaces in addition to the topological
surface states create problems. For (Hg,Cd)Te, the desired
effects are displayed only when the material is buried in
thin‑film heterostructures, limiting the techniques that
can be used to study it. The high vapour pressure of Hg
and the sensitivity of the (Hg,Cd)Te properties to the Hg
content complicate the control of these properties, such
that (Hg,Cd)Te has been fabricated in only a small num‑
ber of laboratories worldwide. By contrast, tetradymites
are perfect materials to begin a large, new field of study —
the crystals are relatively easy to prepare, the topological
physics they display is elegant and new, and the energy
dispersions of the surface states are relatively simple
3–5,9,10
.
Despite their theoretically ideal behaviour, the tetra‑
dymite bulk materials that were initially studied, Bi
2
Se
3
1
Departments of Mechanical
and Aerospace Engineering,
Physics, and Materials
Science and Engineering,
The Ohio State University,
Columbus, Ohio 43210, USA.
2
Department of Chemistry,
Princeton University,
Princeton, New Jersey
08544, USA.
3
Department of Physics and
Materials Research Institute,
the Pennsylvania State
University, University Park,
Pennsylvania 16802, USA.
Correspondence to J.P.H.
heremans.1@osu.edu
doi:10.1038/natrevmats.2017.49
Published online 5 Sep 2017
Tetradymites as thermoelectrics
and topological insulators
Joseph P. Heremans
1
, Robert J. Cava
2
and Nitin Samarth
3
Abstract | Tetradymites are M
2
X
3
compounds — in which M is a group V metal, usually Bi or Sb,
and X is a group VI anion, Te, Se or S — that crystallize in a rhombohedral structure. Bi
2
Se
3
,
Bi
2
Te
3
and Sb
2
Te
3
are archetypical tetradymites. Other mixtures of M and X elements produce
common variants, such as Bi
2
Te
2
Se. Because tetradymites are based on heavy p‑block elements,
strong spin‑orbit coupling greatly influences their electronic properties, both on the surface
and in the bulk. Their surface electronic states are a cornerstone of frontier work on topological
insulators. The bulk energy bands are characterized by small energy gaps, high group velocities,
small effective masses and band inversion near the centre of the Brillouin zone. These properties
are favourable for high‑efficiency thermoelectric materials but make it difficult to obtain an
electrically insulating bulk, which is a requirement of topological insulators. This Review outlines
recent progress made in bulk and thin‑film tetradymite materials for the optimization of their
properties both as thermoelectrics and as topological insulators.
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