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Introduction
Laser surface remelting (LSR) has attracted increasing interest in
recent years owing to its special capabilities. High energy density of
LSR translates into effcient use of energy for remelting, because LSR
modifes surface properties of a material without affecting its bulk
properties. LSR results in rapid quenching of the molten material by
conduction into the cold subsurface after rapid irradiation. This type
of behavior was also observed,
1
who applied laser surface melting
(LSM) technique in a study of high strength aluminum alloys (HSAL).
LSR technique was for a study of hypoeutectic Al-1.5 wt. % Fe
alloy. Characterization of the cast region revealed the formation of
a refned, dense and highly homogeneous microstructure, as well as
cracking, noticeably with a high formation of protuberance on the
weld fllets than alloy untreate.
2,3
An overlapping line of consecutive
weld fllets was also perceptible in the cast region of this alloy, which
resulted in an increase of about 61% in hardness compared to the base
material. The Marangoni effect
4
infuence thermal gradient in the
molten pool a high temperature, meanwhile, also it produces effects in
quality and properties of microstructure, morphological characteristic
and as well as quality of laser-treated workpiece track. Yet these same
authors confrmed, at low laser beam velocities, the morphology is
higher and quality of track presents many defects than at high laser
beam velocities.
Moreover, laser shock peening (LSP) process enables the
improvement of corrosion resistance by means of increased pitting
potential with lower intensity of pitting attack on the specimen’s
surface.
5
Was confrmed higher corrosion resistance of laser-peened
friction stir-welded 7075 aluminum joints in a 3.5% NaCl solution.
6
Although, during LSR-treatment in Al alloy, the melted zone was
constituted of metastable phases by LAXRD analysis and it revealed
the presence mainly of Al
2
O
3
and AlN phases.
2,7
These authors
emphasized, which these phases contributed in the microstructural
modifcation, favored the characteristics of high hardness and
corrosion resistance of LSR-treated work piece in sulfuric acid.
This study involved LSR treatment of hypereutectic Al-2.0 wt.
% Fe alloy. The sample was characterized by various techniques,
including optical microscopy (OM), scanning electron microscopy
(SEM), vickers micro hardness test. Analysis of Vickers hardness
were done in the cross-sectional area of treated sample and on the
treated sample surface. Furthermore, the electrochemical impedance
spectroscopy (EIS) test was studied and their numerical simulation
was done. The microstructure microhardness and electrochemical
behavior of laser-treated layer were systematically investigated to
correlate their properties with process involved.
Materials and methods
Material
Hypereutectic Al-2.0 wt. % Fe alloy under study was prepared with
commercially pure raw materials. The material was cast in a resistance
furnace (muffe) by pouring the liquid metal into a cylindrical ingot
mold and cooling in ascending mode. Resulting ingot was sectioned
into various samples, which were sand blasted individually to
determine the chemical composition of alloy by energy-dispersive
X-ray fuorescence spectrometry (Shimadzu EDX-7000), as indicated
in Table 1.
Adv Tissue Eng Regen Med Open Access. 2018;4(4):103‒110. 103
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Al-Fe alloy processed by laser surface remelting and
your infuence on microstructure, microhardness
and electrochemical behavior
Volume 4 Issue 4 - 2018
Moises Meza Pariona, Katieli Tives Micene,
Alfredo José Zara
State University of Ponta Grossa, Brazil
Correspondence: Moises Meza Pariona, University State
University of Ponta Grossa, Campus Uvaranas - Av. General
Carlos Cavalcanti, 4748 - CEP 84030-900, Brazil, Tel 55-42-
32203056, Email
Received: August 07, 2018 | Published: November 16, 2018
Abstract
An analysis was made of microstructure of hypereutectic Al-2.0 wt% Fe alloy treated
by laser surface remelting (LSR), microhardness test, and electrochemical behavior
test and their numerical simulation was done. Microstructure was analyzed by optical
microscopy, field-emission scanning electron microscopy and Vickers microhardness
tests. Results obtained in this study indicate in LSR-treatment occurred rapid heating
and followed by rapid cooling, resulting in formation of a thin recast layer with a
refined microstructure, with dissolution of precipitates and inclusions and formation
of metastable phases, however, an overlapping line on consecutive weld fillets
was observed. Furthermore, analysis of Vickers hardness were done in the cross-
sectional area of treated sample and on the treated sample surface, therefore, result
a greater microhardness of the treated region than untreated substrate. Through the
electrochemical impedance spectroscopy (EIS) test, laser surface remelting-treated
workpiece exhibit higher polarization resistance than untreated, at 11 times higher and
capacitive behavior of material is related to aluminum oxide layer properties, then,
microstructure characteristic caused by overlapping ratio and multi-track has a strong
effect on electrochemical process. This material can be applied in the aerospace,
autmovolist and implant materials used in medicine.
Keywords: laser surface remelting, Al-2.0 wt.% Fe, microstructure, microhardness,
OM, FESEM, electrochemical behavior
Advances in Tissue Engineering and Regenerative Medicine
Research Article
Open Access