WI
ELSEVIER Chemical Physics 193 (1995)79-87
Chemical
Physics
Adsorption of methanol in zeolite, gallosilicate
and SAPO catalysts
Jumras Limtrakul
Laboratory for Computationaland Applied Chemistry, ChemistryDepartment, Faculty of Science, Kasetsart University,
Bangkok 10900, Thailand
Received 14 June 1994;in final form 8 December 1994
Abstract
Methanol adsorption in zeolite, gallosilicate and silicoaluminophosphate (SAPO) catalysts has been investigated within
the framework of ab initio molecular orbital calculations. Full optimization of all cluster models and their complexes has
been carried out at the DZP/SCF level of theory. Physisorbed methanol and methoxonium cation complexed to the
framework catalyst are found for SAPO catalysts, the latter complexes are observed only at high coverages, while only
hydrogen-bonded physisorbed methanol complexes are obtained for gallosilicates and zeolitic catalysts. The conversion
energy of the hydrogen-bonded physisorbed structure, H3Si-OH-AI(OH)2-O-PH3/[CH3OH]2 to the methoxonium
structure, H3Si-O-AI(OH)2-O-PH3]/[CH3OH~'][CH3OH], is about 6.69 kcal/mol. Comparison with hydrogen halides
and related complexes of methanol shows that protonated SAPO/methanol is a very strong acid.
I. Introduction
The Bronsted acidity of catalysts generated from
surface hydroxyls within their framework is of prime
importance and has been the subject of numerous
theoretical and experimental studies [1-9]. Of partic-
ular interest in this active research is the methanol
conversion to hydrocarbon over zeolitic catalysts,
which is the foundation of certain industrially impor-
tant reactions, i.e. the methanol to gasoline (MTG)
or the methanol to olefin (MTO) processes [10,11].
One of the important steps of these processes in-
volves the methanol adsorption on the catalyst sur-
face. The reaction mechanisms and the nature of
interaction with a zeolitic proton have been the
subject of controversy [12,13].
In this work, the interaction of methanol with
zeolite, gallosilicate, silicoaluminophosphate (SAPO)
catalysts and the protonation of CH3OH by catalytic
protons are investigated by ab initio quantum chemi-
cal calculations on the successful model of
H3SiOH-X(OH)2YH 3 (X = AI, Ga and Y = Si, P)
[14-18] with the aims of: (a) comparing the changes
in structures and bonding of the different framework
structures of catalysts and their complexes, (b) deter-
mining the influence of the structure on the catalytic
properties of zeolites, gallosilicates and SAPO, (c)
investigating the important consequences of methanol
adsorption at low and at high coverages, and (d)
obtaining the reaction energies for methanol desorp-
tion, cluster deprotonation, ion-molecule formation
and the conversion energy of the hydrogen-bonded
physisorbed methanol complexes to methoxonium
cation complexes.
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