Issues in Biological Sciences and Pharmaceutical Research Vol.3(2),pp. 14-20, February 2015
Available online at http://www.journalissues.org/IBSPR/
http://dx.doi.org/10.15739/ibspr.008
Copyright © 2015 Author(s) retain the copyright of this article ISSN 2350-1588
Original Research Article
Eudragit L-100 for enteric coating of hard gelatine
capsules: Formulation and evaluation
Accepted 27 February, 2015
Harith Jameel Mahdi
Department of Applied
Chemistry, Faculty of Applied
Chemistry, University of Samarra,
Iraq.
Author’s E-mail:
ph_harith75@yahoo.com
Tel:+964-7702660991
In an attempt to combine the favourite properties of hard gelatine capsules
with the protective and controlled release properties of enteric coating to
get an appropriately and acceptably formulated enteric coated hard gelatine
capsules with pH dependent drug release characteristic. Two hard gelatine
capsule sizes were selected i.e. size #0 and size #1 in order to test the effect
of capsule size on coating process. Eudragit L-100, a pH dependent solubility
polymer, was tested for suitability for coating of hard gelatine capsules. A
number of formulations with various Eudragit L-100 concentrations were
investigated in order to select the best formula that provides the most ap-
propriate coating properties. A formulations with 3, 5, 6.5 and 10 % (w/w)
Eudragit L-100 were tested. Formula with 6.5 % (w/w) Eudragit L-100 was
selected as it provides a good adhered and continuous coating film with ac-
ceptable disintegration time, dissolution test and excellent stability on
storage for both capsule sizes.
Key words: Hard gelatine capsule, eudragit L-100, enteric coating, direct coating,
and sub-coating.
INTRODUCTION
Since the first development and production of hard gelatine
capsule as pharmaceutical dosage form by Mr. Mothes,
France, in 1834 (Fridrun and Brian, 2004; Katerina et al.,
2010) an annual increases in use and continuous in devel-
opment of new pharmaceutical dosage form using hard
gelatine capsules were recorded (De Carvalho and Grosso,
2006; Sven, 2002). Hard gelatine capsules provides a
unique properties such as fewer manufacturing steps, suit-
ability for poor compaction powder and mostly lower in
manufacturing cost and steps than tablet, (Bussemer and
Bodmeier, 2003; Ashlesha et. al., 2011). In addition to that,
during initial stages of new drug development one of the
most important and sensitive situation is the very limited
quantity of the under investigated active pharmaceutical
ingredient, lack of adequate information about physical and
chemical properties, tight schedule time and with too many
variables that may affects on pharmacokinetic and/or
pharmacodynamic behaviour associated with tablet's
manufacturing (Katerina et al., 2010). All that makes the
hard gelatine capsules to be more favoured dosage form,
suitable and actually preferred in manufacturing of solid
dosage form over tablets. On the other hand, in some cases
like acid sensitive drugs, drugs that irritant to stomach or in
case of drug designed to target a specific site of gastro-
intestinal tract (Ashlesha et al., 2011), hard gelatine
capsules appears to be inappropriate.
The enteric preparations so far frequently used generally
occur as granules, tablets, and capsules filled with enteric
granules (Singh et al., 2012). However, some drugs are not
amenable for production of compressed table but must be
made up into enteric granules or capsules filled therewith
(Jaleh et al., 2012). In such case, it is required that the gran-
ules should be uniform in shape and size (Pallavi et al.,
2010) and so forth so that they can have satisfactory