Far-infrared magneto-optical study of two-dimensional electrons and holes in InAs/Al x Ga 1 x Sb quantum wells J. Kono* and B. D. McCombe Department of Physics, State University of New York at Buffalo, Buffalo, New York 14260 J.-P. Cheng Francis Bitter National Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 I. Lo, § W. C. Mitchel, and C. E. Stutz Wright Laboratory, Wright-Patterson Air Force Base, Dayton, Ohio 45433-6533 Received 6 May 1996; revised manuscript received 15 July 1996 We present results of a detailed far-infrared magneto-optical study on a series of high-mobility InAs/Al x Ga 1 -x Sb x =1.0, 0.8, 0.5, 0.4, 0.2, and 0.1type-II single quantum wells. A wide range of phenom- ena arising from the unusual properties of two-dimensional 2Delectrons and holes and their Coulomb interaction in high magnetic fields has been revealed. Semiconducting samples x 0.4, in which only 2D electrons exist in the InAs wells, exhibit cyclotron-resonance CRsplittings due to large conduction-band nonparabolicity. Semimetallic samples x =0.1 and 0.2, in which both 2D electrons in InAsand 2D holes in Al x Ga 1 -x Sbare present, show two additional lines e and h - X linesas well as electron and hole CR. The X -lines increase in intensity at the expense of CR with increasing electron-hole ( e - h ) pair density, decreasing temperature, or increasing magnetic field at low field, suggesting that they are associated with e - h binding which is increased by the magnetic field. The electron CR shows strongly oscillatory linewidth, amplitude, and mass, part of which are interpreted in the light of the unusual ‘‘antinonparabolic’’ band structure resulting from band overlap and coupling between conduction-band states in InAs and valence-band states in Al x Ga 1 -x Sb; part of these results are qualitatively consistent with the predictions of Altarelli and co-workers. The X lines are attributed to internal transitions of correlated electron e - h pairs excitonsin high magnetic fields mediated by the excess electron density. S0163-18299704403-2 I. INTRODUCTION Semiconductor heterostructures made from the combina- tion of InAs and Al x Ga 1 -x Sb have been of considerable in- terest for the past two decades because of their unusual band- edge alignment, 1 due to which electrons and holes are spatially separated and confined in different layers. Interest in this material system has also been stimulated by the large nonparabolicity, small mass, and large g factor of the elec- trons contained in the InAs layers, compared to commonly used GaAs/Al x Ga 1 -x As systems, as well as possible appli- cations as infrared detectors and sources. Until recently, however, systematic experimental studies of intrinsic proper- ties of this system had been limited to the end member InAs/GaSb, 2 primarily due to the difficulty in growing high- mobility, impurity-free samples. The past several years have seen remarkable progress in the growth of InAs/Al x Ga 1 -x Sb quantum-well QWstructures with high-mobility 10 5 cm 2 /V stwo-dimensional 2Dcarriers. 3–5 This has led to such experimental observations as zero-field spin splitting due to asymmetric potential wells, 6 magnetic-field-induced semimetal-semiconductor transitions, 7–9 cyclotron-resonance CRsplittings due to nonparabolicity, 10,11 strong CR oscillations, 12 far-infrared FIRtransitions attributed to intra-excitonic resonance, 12,13 and magnetic-field-induced spin-conserving and spin-flip intersubband transitions. 14 The unusual band lineups of the Al x Ga 1 -x Sb/ InAs/Al x Ga 1 -x Sb type-II single QW’s under ideal condi- tions with no band bending are schematically depicted in Fig. 1 for three different Al compositions x =0, 0.3, and 1.0. The effective band gap E G * , defined by the energy dif- ference between the lowest electron subband and the highest hole subband, can be varied over a wide range ( -0.15 eV E G * +0.3 eV) by varying x and/or the well width. The end member, GaSb/InAs/GaSb x =0, is a misaligned or broken-gaptype-II ‘‘semimetallic’’ QW. When the well FIG. 1. Schematic conduction solid linesand valence dashed linesband lineups for InAs-Al x Ga 1 -x Sb x =0, 0.3, and 1.0single quantum wells under ideal conditions charge transfer and band bending not included. The ideal system is ‘‘semimetallic’’ when x 0.3 neglecting confinement. PHYSICAL REVIEW B 15 JANUARY 1997-I VOLUME 55, NUMBER 3 55 0163-1829/97/553/161720/$10.00 1617 © 1997 The American Physical Society