Asian J. Research Chem. 4(11): Nov., 2011
1780
ISSN 0974-4169 www.ajrconline.org
RESEARCH ARTICLE
Bioactive Molecule of Onion Leaves Act as Inhibitor of PPO.
A. S. Goswami-Giri* and Neha A. Sawant
B.N. Bandodkar College of Science, Thane-400 601.
*Corresponding Author E-mail: anitagoswami@yahoo.com
ABSTRACT:
Bioactive molecules of onion leaves exhibited potent anti polyphenol oxidase (PPO) activity; which was purified on
silica gel by using solvents. Purification profile procured 3 and 2 active butanol and methanol fractions respectively.
Reticence of PPO activity was observed within range of 12 to 14 min when it was treated with active fractions.
Characterization of it was conceded by physical constant, UV, IR and TLC. It reputes that, active hydroxyl group
attached to the ring structures of PPO, which quench free radical by donating hydrogen in the active hydroxyl group of
PPO, confirming inhibition of pigmentation reaction in vitro. Bioactive molecules from onion leaves exhibited various
types of inhibition against oxidation of L-DOPA and L-tyrosine and it was compared with classical inhibitors of PPO.
Significance of bioactive molecules is to explore for drugs designing, understanding of ligand–receptor interactions,
environmental problems and it is simple alternative for the inhibition of PPO.
KEYWORDS: Onion leaves; quercetin; oxazolone; flavanoid; cinnamic acid; inhibition.
INTRODUCTION:
Onion and onion leaves is essential ingredient of vegetarian
and non-vegetarian diets having medicinal and nutritive
value. Though onion is useful, onion leaves turn black when
cut, due to oxidation of 3, 4-dihydroxyphenylalanine (dopa)
to pigmented products. This reaction is catalyzed by group
of enzymes; polyphenol oxidase (PPO). Pigmentation is
often an undesirable reaction, which is responsible for
unpleasant sensory qualities, significant loss in nutritional
qualities and market value of fruits/vegetables. The
prevention of this reaction has always been a challenge to
food scientist
1
. Discrimination of this reaction is
responsible for various types of diseases and disorders viz
Parkinsonia
2
, albinism, melanoma, psychological effect-
schizophrenia
3,4
, gastrointestinal side effects and melanin-
based bias in human societies.
In India, Maharashtra is the major place where fruits and
vegetable are cultivated on a large scale but in peak season
if transport facilities become unavailable, fruits and
vegetable being perishable, leads to economic loss to the
farmers. Consequently change in color is a major problem.
Many inhibitors are often used to prevent the pigmentation,
which are toxic to human beings.
Received on 16.09.2011 Modified on 03.10.2011
Accepted on 18.10.2011 © AJRC All right reserved
Asian J. Research Chem. 4(11): Nov., 2011; Page 1780-1783
Therefore searching for nontoxic inhibitors having broad
application for these activities is important in developing a
rational chemotherapy of pigmentation. In the present
paper, the biologically active compounds from onion leaves
extracted by using organic solvent were bioassay for
inhibitory effect. Bioactive conformation of drugs is one of
the key points for understanding the ligand–receptor
interactions
5
. Therefore, the Onion leaves organic extract
was purified on silica gel. Fractions were characterized by
physical constant, TLC, UV and IR spectra.
MATERIALS AND METHODS:
Materials:
L-dopa, l-tyrosine, sodium phosphate (mono and dibasic),
ammonium sulfate, citron X-100, EDTA, ascorbic acid
were obtained from E. Merck (India). Sephadex G-25 from
pharmacia, silica gel ammonium hydroxide, di-ethylether ,
chloroform, acetone from Loba Chemicals, butanol from
SRL. Other chemicals used were of analytical pure grade.
Methanol was obtained locally and was distilled prior to
use.
Source:
Fresh onion leaves were obtained directly from the fields,
were washed and then stored at 4°C in a refrigerator for
about 24 hrs.
PPO extraction from onion leaves by solvent and salt
method:
Fresh onion leaves (300 g) were homogenized with 150 ml
of ice-cold acetone, water with Citron X-100 (80:19:1,