Research Article 2017, 2(9), 596-601 Advanced Materials Proceedings
Copyright © 2017 VBRI Press 596
Self-assembling nano films on metal surface
as corrosion inhibitors
Susai Rajendran
1
, R Joseph Rathish
2
and S Santhana Prabha
2
1
Corrosion Research Centre, Department of Chemistry, St Antony’s College of Arts and Sciences for Women,
Amala Annai Nagar, Thamaraipadi, Dindigul, Tamilnadu, 624 005, India
2
PSNA College of Engineering and Technology, Dindigul, Tamilnadu 624622, India
*
Corresponding author: Email: suasirajendran@gmail.com, rathishjoseph@gmail.com; Tel: +91 (0) 9443631628
Received: 30 March 2016, Revised: 02 October 2016 and Accepted: 17 April 2017
DOI: 10.5185/amp.2017/650
www.vbripress.com/amp
Abstract
Self-assembling molecules form protective layers on metal surfaces Self assembled nanofilms of adipic acid, N-
cetyl-N,N,N-trimethyl ammonium bromide, Tween- 60, Sodium dodecyl sulphate and an aqueous extract of banana
peel have been formed on the surface of carbon steel by the immersion method. The formation of the nanofilms
has been confirmed by Fourier Transform Infrared spectral study and Atomic Force Microscopy Study. The
corrosion inhibitive nature of the protective film has been estimated by the classical weight loss method and
electrochemical study such as polarization study. The hydrophobic nature of the protective film has been
investigated by measurement of contact angles of the protective films. The hydrophobic surfaces may find
application in various exciting fields such as corrosion protection, raincoats, water proof surfaces and biomaterials.
Copyright © 2017 VBRI Press.
Keywords: Self assembling nanofilm, corrosion inhibition, hydrophobic surfaces, AFM, FTIR, contact angle
measurement, hydrophobicity.
Introduction
Corrosion can be considered as a natural process.
This spontaneous process is thermodynamically
favorable. The rate of corrosion can be controlled by
many methods. Use of corrosion inhibitors is one
such method. These inhibitors may be classified as
anodic type, cathodic type or mixed type. This
classification depends on whether they control anodic
reaction or cathodic reaction or both type of
reactions, predominantly. A good inhibitor is
expected to be water soluble and hydrophobic (to
displace water from metal surface). The corrosion
inhibitors should have a good delivery mechanism
also.
Nanotechnology is one of the hottest fields, which
draws attention from all over the world and has the
potential to outdate most of the technology existing
today. Nanomaterials are very important because they
have very special properties which may lead to new
and exciting application including corrosion control
[1]. Nanoparticles-based corrosion inhibitors offer
better corrosion protection efficiency than the
ordinary ones, because as the size of the particle
decreases the surface area for a given mass and hence
the number of active centers increases. Finally, this
leads to efficient chemisorptions/physisorption of
nanosized inhibitors on corroding metal surfaces. So,
enhanced corrosion inhibition efficiency can be
realized where nanoparticles/nano films are used as
corrosion inhibitors.
Self-assembling nanofilms can be formed on the
metal surface or metal oxide surface by various
techniques which include simple immersion method
in a suitable solvent containing the molecules to be
assembled on the metal surface. Molecules can be
assembled on nickel [2- 9], which is a key component
in the electronic industry and an important alloying
constituent in many biometrials. Self-assembling
nanofilm can be formed on copper surface [10-14]
and carbon steel surfaces [15,16].
Self-assembling nanofilms have many potential
applications in many areas such as non-wetting
surface, corrosion inhibition, lubrication, monolayer
lithography, biocompatible surfaces,etc [17-19]. Self-
assembling nano layers are found to be hydrophobic
and hence prevent water molecules reaching the
metal surface. Hence corrosion of metals is prevented
by self-assembled nano films formed on metal
surface. The water repelling nature of nano layers can
be compared with “Lotus Effect”, wherein water
droplets rolled down the lotus leaves whereby self-
cleaning effect also takes place.