Global Advanced Research Journal of Microbiology (ISSN: 2315-5116) Vol. 3(8) pp. 133-143, October, 2014
Available online http://garj.org/garjm/index.htm
Copyright © 2014 Global Advanced Research Journals
Full Length Research Paper
Synthesis, spectroscopic, Thermal kinetic and
computational studies on Charge-Transfer Complexes:
(Panto & Ome)-prazole drug as donor and DDQ, CHLC &
Iodine as acceptor
Doa'a Fawzi Ba'amer
1
, Elsayed El-Mossalamy
2
, Laila Mohammad Al-Harbi
1*
, Abdullah Yousif
Obaid
1
1
Department of Chemistry, Faculty of Science, King Abdulaziz University, P.O. Box 42805 Jeddah 21551 Saudi Arabia.
2
Department of Chemistry, Faculty of Science, Benha University, Benha, Egypt.
Accepted 10 October, 2014
Charge transfer (CT) complexes were carried out using the most widely selling and effective
pharmaceutical drugs as Pantoprazole (PANT) and Omeprazole (OMER) as electron donors; solid
interaction with different benzoquinone derivatives as acceptors and Iodine were isolated and
characterized by IR and
1
H-NMR (Nuclear magnetic resonance) .Thermo gravimetric analysis with
different heating rates (TGA) were studied on solid state complexes using computational integral
methods for Coats Redfern and Ozawa using various solid state kinetic reaction models and established
activation energy, energy band gape and thermodynamic parameters . The Differential Scanning
Calorimetric (DSC) technique was used to study the nature decomposition of charge transfer complexes.
The morphological structure were discussed and examined via Scanning Electron Microscopy (SEM).The
molecular structures of Pentaprazole, DDQ, CHLC and I
2
& charge transfer complexes in the ground state
were made by using Gaussian 03 program package.
Keyword: thermal kinetic studies, pharmaceutical drugs, benzoquinone derivatives, Computational chemistry.
INTRODUCTION
Mulliken was the first who introduced the charge transfer
phenomena (Mulliken 1952). The organic charge transfer
complexes were intensively investigated due their
application in many biological fields, solar energy storage,
surface chemistry and their uses in quantitative estimation
of drugs[2].In this study Omeprazole (OMER) {5-Methoxy-
2[[ 4- methoxy-3, 5-dimethyl-2-pyridinyl ]sulfinyl] - 1H-
*Corresponding Author's Email: sbdmina@yahoo.com;
Tel: +20-1009143680.
benzimidazole} and Pantoprazle (PANT).
{5-(Difluoronylmethoxy)-2-[[3,4-dimethoxy-2
pyridnyl)methyl]sulfinyl]-1H-benzimidazole}, in the form of
{pantoprazole sodium sesquihydrate}, are two irreversible
proton pump inhibitors (PPIs) are used as donors with
benzoquinone derivatives as acceptors and Iodine. The
formed charge transfer complexes are synthesized and
characterized by mid infrared spectroscopy, elemental
analysis, and proton magnetic resonance
1
HNM.Thermal
studies were characterized by using thermogravimetric
analysis (TGA) and differential scanning calorimetry (DSC).