Pore-size tuning in double-pillared metal-organic frameworks
Containing Cadmium clusters
Zu-Jin Lin, Tian-Fu Liu, Bo Xu, Li-Wei Han, Yuan-Biao Huang, and Rong Cao*
State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of
Matter, Chinese Academy of Sciences, Fujian, Fuzhou, 350002, China
Contents
1- General experimental methods S2
2- Typical procedures for the preparation of H
8
X ligand S3
3- Synthesis of materials S4-S15
4- Powder X-Ray Diffraction S15-S17
5- Thermogravimetric Analysis (TGA) S17-S20
6- X-ray Crystallography of compounds 1-4 S20
7- Additional figures and Scheme S21-S24
*Author to whom correspondence may be addressed: rcao@fjirsm.ac.cn
Supplementary Material (ESI) for CrystEngComm
This journal is © The Royal Society of Chemistry 2011