Please cite this article in press as: F.X. Qin, et al., Effects of wire properties on the field-tunable behaviour of continuous-microwire composites,
Sens. Actuators A: Phys. (2012), doi:10.1016/j.sna.2012.02.011
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Effects of wire properties on the field-tunable behaviour of
continuous-microwire composites
F.X. Qin
a,∗
, H.X. Peng
a
, M.H. Phan
b
, L.V. Panina
c,d
, M. Ipatov
d
, A. Zhukov
d
a
Advanced Composite Centre for Innovation and Science, Department of Aerospace Engineering, University of Bristol, University Walk, Bristol BS8 1TR, UK
b
Department of Physics, University of South Florida, Tampa, FL 33620, USA
c
School of computing, Communication and Electronics, University of Plymouth, Drake Circus, Plymouth, Devon PL4 8AA, UK
d
Dpto. de Fisica de Materiales, Fac. Quimicas, Universidad del Pais Vasco, Bilbao, San Sebastian 20009, Spain
a r t i c l e i n f o
Article history:
Received 1 September 2011
Received in revised form 9 February 2012
Accepted 9 February 2012
Available online xxx
Keywords:
Field tunable properties
Continuous microwire composites
Ferromagnetic microwires
Plasma frequency
Self-sensing application
PACS:
78.55.Qr
62.23.Pq
87.15.La
a b s t r a c t
The microwire composites consisting of continuous Co-rich amorphous glass-coated ferromagnetic
microwires embedded in a E-glass prepreg matrix were fabricated, and the influences of wire period-
icity (b), composition and radius on the field-tunable properties have been systematically investigated
in a broad microwave frequency range of 0.9–18 GHz. It has been found that the field tunability, effec-
tive operational frequency and field of the composites are strongly dependent on these factors. With
decreasing b from 15 to 7 mm, the field tunability of effective permittivity (n
ε
) increases from 0.77% to
16% m/A by more than 20 times. The detected cups and resonances of the transmission and reflection
spectra are identified. Their changes with wire periodicity have been shown to be due to a combination of
the dielectric and magnetic response arising from the interactions between microwave and microwires
and microwires by themselves. The best possible field tunability occurs below the plasma frequency.
The effective magnetic field for realisation of the field-tunable properties has been found to be about
500 A/m, which is associated with the anisotropy field. In addition, field tunability is found to be posi-
tively correlated with the magnetic softness and GMI properties of the wire fillers, which are determined
by the wire composition and geometry. These findings are of practical importance in developing multi-
functional microwire composites for a broad range of engineering applications, such as structural health
monitoring, NDT and microwave tunable devices.
© 2012 Elsevier B.V. All rights reserved.
1. Introduction
Introducing additional functionalities into a structural com-
posite material for specific purposes of domestic and engineering
applications is an area of topical interest [1–4]. Particular atten-
tion has been paid to “multifunctional” composites that, beyond
their essential structural function, possess other functionalities
achieved by constituent materials in an optimised structure. While
the electromagnetic functionality has been extensively explored in
a variety of complex composites [5–9], the recent progress in devel-
oping new composites with superior microwave tunable properties
indeed affords them for a broad range of applications from the
high-performance frequency selective surfaces and the self-sensing
media for the remote non-destructive test of structural materials
to tunable filters and phase shifters [10–14]. This type of com-
posites consists of conductive scattering elements embedded in a
∗
Corresponding author. Now at: Lab-STICC, Université de Bretagne Occidentale,
CS 93837, 6 Avenue Le Gorgeu, 29238 Brest Cedex 3, France. Tel.: +33 2 98 01 80 09;
fax: +33 2 98 01 61 31.
E-mail address: faxiang.qin@gmail.com (F.X. Qin).
dielectric matrix. It has been shown that the composite is irradiated
by electromagnetic wave and its dielectric response characterised
by the complex effective permittivity depends intimately on the
impedance of the fillers [15]. The fillers are therefore required to
possess a somewhat unique property ensuring a sensitive response
to the electromagnetic excitation such as giant magneto-/stress-
impedance effect (GMI/GSI), which is defined as a large variation
of the high frequency impedance caused by an applied magnetic
field/stress. As a result, the dispersion characteristics of the effec-
tive permittivity depend on magnetic field and/or stress.
In order to realise the tunable properties, the following condi-
tions concerning the constituents of the composites are prioritised
[16]: (i) the fillers should possess GMI effect and good soft magnetic
property; (ii) the fillers are also preferred to have large permit-
tivity and good conductivity to ensure strong dielectric responses
of the composite to the electromagnetic wave. Following these
criteria, the Co-based ferromagnetic microwires exactly meet the
requirements. They have a unique circular magnetic anisotropy due
to coupling between the negative magnetostriction and frozen-in
stress. Such anisotropy is important to realise a large and sensitive
magnetoimpedance (MI) effect for applications in miniature mag-
netic sensors [17]. In addition, its fine size guarantees a minimal
0924-4247/$ – see front matter © 2012 Elsevier B.V. All rights reserved.
doi:10.1016/j.sna.2012.02.011