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International Journal of Scientific Research in Science, Engineering and Technology
Print ISSN: 2395-1990 | Online ISSN : 2394-4099 (www.ijsrset.com)
doi : https://doi.org/10.32628/IJSRSET229227
181
Adhesive less Silica Nanoparticle Coating on Nylon Woven Fabric
and Its Characterization
Afsana Sharmin
1
, Kazi Md Hasanul Hoque
2
, Zhang Huapeng
*
Zhejiang Sci-Tech University, Hangzhou-310018, China
Article Info
Volume 9, Issue 2
Page Number : 181-191
Publication Issue :
March-April-2022
Article History
Accepted: 15 March 2022
Published: 06 April 2022
ABSTRACT
Environment-friendly functional woven fabric with light weight has higher
market demand in this era. This paper is aimed to prepare and characterize
super-hydrophobic nylon-6 woven fabric by using silica nanoparticles,
coupling agent 3-aminopropyltriethoxysilane (APTES), and a long chain
hydrophobic agent hexadecyltrimethoxysilan (HDTMS). Synthesize of silica
nanoparticles is processed with a modified Stöber method resulting in a mono-
dispersed particle whose diameter is 51-60 nm. In this experiment chemical
bonds presenting over the surface silica nanoparticle are Si–CH3 and Si-OH
Due to the reaction between the hydrolyzed APTES and the first layered
surface, the Si-OH group is spectra onto the surface. The hydrolyzed HDTMS
molecules created a bond to the surface by the formation of Si–O–Si bonds. As
result, a long chain of organo-silane with low surface free energy is introduced
onto the fabric surface. The hydrophobic coated surface appeared after spray
coating with additional treatment without any adhesive. The super-
hydrophobic nylon-6 woven fabric has been coated by spray method with
static water contact angle 151.8֯. Characterization manifests a good self-
cleaning tendency and low permeability difference.
Keywords: Silica nanoparticles, Nylon-6 woven fabric, super-hydrophobic,
coating, synthesis, Stöber method.
I. INTRODUCTION
Consumer demand for a comfortable and healthy lifestyle at the same time in one certain product has created
the concept of multi-functional textiles. Hydrophobicity, air permeation, soil release tendency, and mostly
lightweight clothes, etc. are in high demand of the market, and in current decades the attraction raises of
hydrophobic or super-hydrophobic fabrics. Hydrophobic surfaces are characterized by a water contact angle of
90֯ to 150֯ and for super-hydrophobic is greater than 150 ֯ [1]. “Lotus leaf” which constitutes the hydrophobic
epicuticular wax (decrease surface wetting) associated with the micro or nano-scale stratified architectures has
made the concept of ultra-hydrophobic or super-hydrophobic [2]. Proper micro or nanostructures to create
surface roughness and materials with low surface energy in a combined form can produce a super-hydrophobic