J. Nanoanalysis., 6(1): 48-56, Winter 2019
RESEARCH ARTICLE
Electrodeposi ton of anionic, catonic and nonionic surfactants and
gold nanopartcles onto glassy carbon electrode for catechol detecton
Maryam Nazari
1,3
, Soheila Kashanian
2,3,
*, Rezvan Mohammadi
1
1
Faculty of Chemistry, Razi University, Kermanshah, Islamic Republic of Iran
2
Faculty of Chemistry, Sensor and Biosensor Research Center (SBRC) and Nanoscience and Nanotechnology
Research Center (NNRC), Razi University, Kermanshah, Islamic Republic of Iran
3
Nano Drug Delivery Research Center, Faculty of Pharmacy, Kermanshah University of Medical Sciences,
Kermanshah, Iran
Received: 2018-10-01 Accepted: 2018-11-28 Published: 2019-02-01
ABSTRACT
Three surfactants were selected to modify glassy carbon electrode including sodium
dodecylbenzenesulfonate, Tween 80 and cetyltrimethylammonium bromide. The obtained nano-
Au/surfactant/GCEs were characterized with scanning electron microscopy and electrochemical
techniques. Electrochemical behavior of catechol at the nano-Au/surfactant/GCE was thoroughly
investgated for modifed electrodes. Compared to the unmodifed electrode, the peak current
obviously increased and the oxidaton and reducton peaks potental shifed to the negatve and
positve potental area, respectvely, meaning the peak potental separaton is reduced. These
changes indicated that the composite nanopartcles possess good electrocatalytc performance on
the electrochemical reacton of catechol. The experimental results revealed that the nanopartcle
modifed electrodes have good performances for catechol sensing, which including convenient
fabricaton, low detecton limits and wide linear ranges. These merits of this sensing system provide
high potental to apply in environmental monitoring. In additon, kinetc parameters of catechol
redox reacton were determined and the number of electrons was obtained two for the three
modifed electrodes.
Keywords: Catechol; Cetyltrimethylammonium Bromide; Gold Nanopartcle; Sodium Dodecylbenzene
Sulfonate; Tween 80
© 2019 Published by Journal of Nanoanalysis.
How to cite this artcle
Nazari M, Kashanian S, Mohammadi R. Electrodepositon of anionic, catonic and nonionic surfactants and gold
nanopartcles onto glassy carbon electrode for catechol detecton. J. Nanoanalysis., 2019; 6(1): 48-56.
DOI: 10.22034/jna.2019.664401
ORIGINAL RESEARCH PAPER
Tis work is licensed under the Creative Commons Attribution 4.0 International License.
To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.
* Corresponding Author Email: kashanian_s@yahoo.com
INTRODUCTION
A large variety of phenolic compounds are
widely used in the manufacture of products,
including coal conversion, petroleum refning,
pharmaceuticals, production of dyes, pesticides,
resins, and plastics and thus readily release into the
ground and surface water [1-3]. Te identifcation
and quantifcation of these compounds are
important for environmental monitoring because
many of them are toxic contaminants in medical,
food and environmental matrices and have
harmful efects on plants, animals and human
health [4-6]. Te maximum amount of phenols in
wastewater allowed by the European Community
is lower than 1 ppm [7]. Many analytical methods
are available for the determination of them, such as
spectrophotometry, chromatography, and capillary
electrophoresis. However, these methods are time-
consuming and the instrumentations are expensive
[8,9]. Sensors can provide ideal sensing systems