Effect of equal channel angular pressing (ECAP) on
hydrogen storage properties of commercial
magnesium alloy AZ61
Song-Jeng Huang
a,*
, Chun Chiu
a
, Tun-Yu Chou
a
, Eugen Rabkin
b
a
Department of Mechanical Engineering, National Taiwan University of Science and Technology, No. 43, Keelung
Rd., Sec. 4, Da'an Dist., Taipei, Taiwan, ROC
b
Department of Materials Science and Engineering, Technion e Israel Institute of Technology, Technion City, Haifa
3200003, Israel
article info
Article history:
Received 3 September 2017
Received in revised form
5 January 2018
Accepted 8 January 2018
Available online xxx
Keywords:
Hydrogen storage
Equal channel angular pressing
(ECAP)
Gravity casting
AZ61 magnesium alloy
abstract
Cast commercial AZ61 magnesium alloys were processed through equal channel angular
pressing (ECAP) and were comminuted into chips by filing with a rasp in order to measure
their hydrogen storage properties. The effects of the number of ECAP passes and the
processing route of ECAP on the hydrogen storage properties of AZ61 magnesium alloys
were investigated. ECAP processing led to severe dynamic recrystallization and grain
refinement of the AZ61 alloys. Of the analyzed samples, the AZ61 alloy processed via the Bc
ECAP route with eight passes exhibited the smallest grain size, the fastest hydrogen ab-
sorption and desorption rates, and the highest gravimetric hydrogen storage capacity of
6.2 wt%.
© 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.
Introduction
Hydrogen is considered a viable environmentally friendly
alternative to fossil fuels for application in the automotive
industry. Moreover, it is considered a promising energy carrier
for future energy systems. However, the widespread use of
hydrogen is impeded by its storage technology, especially for
application in vehicles powered by fuel cells and in hydrogen-
fueled internal combustion engines. Hydrogen stored in metal
hydride materials exhibit advantageous characteristics such
as a high volumetric storage capacity and intrinsic safety [1,2].
Metal hydrides have been considered a hydrogen storage so-
lution with performance comparable with that of other stor-
age options (e.g., high pressure tanks, liquefaction).
To this end, among metal hydrides, magnesium hydride
(MgH
2
) is one of the most attractive candidates because of its
high theoretical gravimetric capacity of 7.6 wt%, reversible
hydrogen release and uptake, and relatively low cost. MgH
2
has the highest hydrogen content and hence the highest en-
ergy density (9 MJ/kg of Mg) of all reversible hydrides suitable
for hydrogen storage. The disadvantages of MgH
2
as a
hydrogen storage material are the relatively large amount of
heat required to release hydrogen, slow hydrogen absorption
* Corresponding author.
E-mail address: sgjghuang@mail.ntust.edu.tw (S.-J. Huang).
Available online at www.sciencedirect.com
ScienceDirect
journal homepage: www.elsevier.com/locate/he
international journal of hydrogen energy xxx (2018) 1 e10
https://doi.org/10.1016/j.ijhydene.2018.01.044
0360-3199/© 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.
Please cite this article in press as: Huang S-J, et al., Effect of equal channel angular pressing (ECAP) on hydrogen storage properties of
commercial magnesium alloy AZ61, International Journal of Hydrogen Energy (2018), https://doi.org/10.1016/j.ijhydene.2018.01.044