Phase Behavior and Structure of Ternary Amphiphilic
Block Copolymer-Alkanol-Water Systems: Comparison of
Poly(ethylene oxide)/Poly(propylene oxide) to
Poly(ethylene oxide)/Poly(tetrahydrofuran) Copolymers
Peter Holmqvist,* Paschalis Alexandridis, and Bjo ¨rn Lindman
Physical Chemistry 1, Center for Chemistry and Chemical Engineering, Lund University,
P.O. Box 124, S-221 00 Lund, Sweden
Received August 16, 1996. In Final Form: December 30, 1996
X
The phase behavior of amphiphilic copolymer-alkanol-water ternary systems was investigated for
triblock copolymers of similar molecular weight and the same hydrophilic block [poly(ethylene oxide), E]
but having different hydrophobic blocks [poly(propylene oxide), P, or poly(n-butylene oxide) ) poly-
(tetrahydrofuran), T]. The alkanol used (butan-1-ol) was comparable in terms of chemical composition to
the hydrophobic segments. A rich phase behavior was obtained for the polymer with the P middle block
(Pluronic F127, E
100P70E100): five different one-phase regions, i.e., micellar (L1) and reverse micellar (L2)
solutions, and (micellar) cubic (I1), hexagonal (H1), and lamellar (LR) lyotropic liquid crystalline regions,
were detected. The microstructure in the liquid crystalline regions was established from small-angle
X-ray measurements; I
1 was found to be primitive cubic. The alkanol molecules are most likely anchored
with their OH- group at the E-P interface, increasing the apparent volume of the P blocks relative to
that of the E blocks, and thus causing a decrease in the polymer layer curvature from spherical to cylindrical.
Only a single one-phase region, extending from the water to the alkanol corner, was observed in the
E
100T27E100 ternary phase diagram. The extent of the one-phase regions decreased for both E100T27E100
and E100P70E100 systems when the alkanol molecular weight increased.
Introduction
Amphiphilic copolymers, and in particular triblock
copolymers consisting of a poly(propylene oxide) (P) middle
block and poly(ethylene oxide) (E) end blocks (com-
mercially available under the Pluronic and Synperonic
trade names and also known as poloxamers), exhibit a
very interesting solution behavior and have been the
subject of many recent studies (see refs 1-4 for reviews).
Block copolymers of the E
n
P
x
E
n
type behave in aqueous
solutions in many respects like typical non-ionic sur-
factants: they are surface active,
5
P being hydrophobic
and E hydrophilic, and can form different self-assembled
structures (micellar solutions
6,7
as well as cubic, hexagonal,
and lamellar lyotropic liquid crystals
8-11
) depending on
the polymer concentration and/or temperature. The
characteristic length and time scales related to self-
assembly are usually larger than those of typical surfac-
tants, since the amphiphilic block copolymers are 10 to 30
times bigger. An advantage of this class of “surfactants”,
when compared to typical nonionic surfactants, is the great
control over the amphiphilic properties afforded by the
variation (during synthesis) of the size and the ratio
between the hydrophobic and the hydrophilic blocks;
12
this is especially important in the various applica-
tions.
4,13,14
Moreover, poloxamer-type block copolymers
exhibit low toxicity
15
and are thus used in pharmaceutical
products.
14
Block copolymers consisting of poly(ethylene
oxide) and poly(1,2-butylene oxide) (B)
16,17
or poly(n-
butylene oxide) (also called polytetrahydrofuran, T, be-
cause of the monomer used for their synthesis)
18
are also
surface active and self-assemble in solution but are less
studied than the E
n
P
x
E
n
copolymers; E
n
B
x
E
n
copolymers
became commercially available only recently.
16
Although the aqueous solution behavior of E
n
P
x
E
n
-type
amphiphilic block copolymers is well studied
1-3
relatively
little is known about their ternary systems with water
and organic solvents.
19-22
The hydrophobic blocks of the
E
n
P
x
E
n
,E
n
B
x
E
n
, and E
n
T
x
E
n
amphiphilic copolymers differ
in polarity from those commonly found in nonionic sur-
factants: in the P, B, and T blocks there is a lot of ether
oxygen present which imparts polarity, while the hydro-
phobic part of nonionic surfactants is usually an alkyl
chain. Because of this polar character, it is not possible
to dissolve aliphatic hydrocarbons (which are often
encountered in mixtures with nonionic surfactants
23
) in
X
Abstract published in Advance ACS Abstracts, March 1, 1997.
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