117
Mater. Res. Soc. Symp. Proc. Vol. 1299 © 2011 Materials Research Society
DOI: 10.1557/opl.2011.59
Film Conductivity Controlled Variation of the Amplitude Distribution
of High-temperature Resonators
Silja Schmidtchen, Denny Richter, Han Xia and Holger Fritze
Institute of Energy Research and Physical Technologies and Energy Research Center
Niedersachsen, TU Clausthal, 38640 Goslar, Germany
ABSTRACT
High-temperature measurements of the spatial distribution of the displacement
characteristics of a thickness shear mode langasite (La
3
Ga
5
SiO
14
) resonator are obtained using a
laser Doppler interferometer. Thereby, the resonator is excited in the fundamental mode and the
third overtone. Further, the resonator is coated with a gas sensitive CeO
2-x
film which exceeds
the metal electrode. In reducing atmospheres the conductivity of the film increases and induces
an increase of the effective electrode area. This effect leads to a broadening of the mechanical
displacement distribution. The latter depends strongly on the size of the excited part of the
resonator which is determined by the effective size of the electrodes. The direct determination of
the mechanical displacement at different oxygen partial pressures confirms a model as derived
from the electrical impedance of resonator devices [1]. Further, information about the mass
sensitivity distribution of resonators is obtained since the property is directly proportional to the
amplitude.
INTRODUCTION
High-temperature stable langasite resonators can be used to determine atmosphere-
induced changes in the mechanical and electrical properties of metal oxide films at elevated
temperatures [1]. Potential devices include gas sensors for high-temperature applications
showing an increased selectivity to different reducing gases like H
2
and CO in comparison to
conventional conductivity based metal oxide sensors [2]. Alternatively, piezoelectric transducers
can be used to study the electrical and visco-elastic properties of metal oxides under different
conditions [3]. In the presented work, the principles of the conductivity-induced variation of the
effective electrode diameter and its influence on the distribution of the mechanical displacement
of piezoelectric resonators are determined and discussed.
For this purpose a CeO
2-x
film is applied on top of the metal electrode of the resonator.
Since the area of the CeO
2-x
film is larger than the metal area, a change in the conductivity of the
film causes a change of the effective electrode area and therefore of the excited area of the
resonator. The spatial distribution of the displacement amplitude and, thereby, of the mass
sensitivity depends on the size of the excited part of the resonator as shown schematically in
FIGURE 1.