Instabilities Across the Isotropic Conductivity Point in a Nematic Phenyl Benzoate under AC Driving Pramoda Kumar, Shivaram N. Patil, Uma S. Hiremath, and K. S. Krishnamurthy* ,† Centre for Liquid Crystal Research, P. O. Box 1329, Jalahalli, Bangalore 560 013, India, and Garden City College, Virgonagar Post, Bangalore 560 049, India ReceiVed: April 5, 2007; In Final Form: May 14, 2007 We characterize the sequence of bifurcations generated by ac fields in a nematic layer held between unidirectionally rubbed ITO electrodes. The material, which possesses a negative dielectric anisotropy ǫ a and an inversion temperature for electrical conductivity anisotropy σ a , exhibits a monostable tilted alignment near T IN , the isotropic-nematic point. On cooling, an anchoring transition to the homeotropic configuration occurs close to the underlying smectic phase. The field experiments are performed for (i) negative σ a and homeotropic alignment, and (ii) weakly positive σ a and nearly homeotropic alignment. Under ac driving, the Freedericksz transition is followed by bifurcation into various patterned states. Among them are the striped states that seem to belong to the dielectric regime and localized hybrid instabilities. Very significantly, the patterned instabilities are not excited by dc fields, indicating their possible gradient flexoelectric origin. The Carr-Helfrich mechanism-based theories that take account of flexoelectric terms can explain the observed electroconvective effects only in part. Introduction The response of a nematic fluid to an external electric field is determined by several factors relating to material and field parameters, and the sample configuration. Much of the vast literature devoted to electrically driven instabilities in nematics dwells on one or the other of two different phenomena: First, purely orientational equilibrium effects such as caused by dielectric anisotropy, flexoelectric polarization and surface polarization; second, nonequilibrium dissipative effects, as found in the vortical flows attributable to anisotropic electrical conduction, charge injection at the electrodes or surface charge inhomogeneity. 1-4 Situations involving interplay of different bifurcation mechanisms are of particular relevance to nonlinear science and, in recent years, a few significant studies have been conducted in this area. For instance, Delev et al. 5 have reported their experimental and theoretical results concerning the cross- over between flexoelectric and electroconvective distortions occurring in a homeoplanar nematic subject to a dc field. Similarly, Dressel et al. 6 have demonstrated the coupling of homogeneous and vortex modes to generate the so-called splay and twist normal rolls. More recently, Dressel and Pesch 7 have reported their rigorous theoretical analysis of the competition between electroconvection (EC) and the Freedericksz effect (FE), and we have discussed the experimental results relating to this competition. 8 In this paper, we report mainly on some hybrid electroconvective instabilities arising within the Freed- ericksz distorted state of a nematic. Nematic EC due to anisotropic material parameters is principally governed by ǫ a ) (ǫ | - ǫ ) and σ a ) (σ | - σ ), | and denoting the directions relative to the nematic director n. Nematics with negative ǫ a , positive σ a , and planar alignment p, conveniently referred to as (-+ p) compounds, taken between ITO-coated glass plates and driven by a field along the substrate normal, are established as the ideal candidates to exhibit a well ordered sequence of hydrodynamic instabilities, starting with periodic rolls at a threshold voltage and developing into chaotic flows far from equilibrium. 9 These classic instabili- ties are understood essentially on the basis of the so-called Carr-Helfrich (CH) mechanism that addresses, for the applied dc field, the coupling between σ a and the bend curvature distortion leading to periodic space charges of alternating sign along the initial director. The body force due to these charges sets up periodic cellular flows above a voltage threshold V c , which, in turn, is determined by the balance between the destabilizing hydrodynamic and transverse-field torques, and the stabilizing dielectric and elastic torques. The corresponding one-dimensional (1-D) analysis for an ac field of frequency ω predicts 10 the instability threshold field E c (ω) to be where k 33 denotes the bend elastic constant, λ the period of stripes, τ the charge relaxation time, and 2 the Helfrich parameter; R 2 and η 1 are the Leslie and Miesowicz viscosity coefficients, respectively. The cutoff frequency ω c ) ( 2 - 1)/τ defines the limit of the conduction regime within which the space charges oscillate at the field frequency while the director pattern is static. Beyond ω c , in the dielectric regime, the space charges are static, but the director oscillates. The occurrence of instability in either regime requires ( 2 - 1) to be positive. Goscianski and Leger 11 were perhaps the first to consider the effect of varying ( 2 - 1) between positive and negative values via temperature dependent σ a in nematics with an * Corresponding author. E-mail: murthyksk@gmail.com. Centre for Liquid Crystal Research. Garden City College. E c 2 (ω) ) ǫ | k 33 λ 2 (1 + ω 2 τ 2 ) ǫ o ǫ a ǫ (1 + ω 2 τ 2 - 2 ) ; 2 ) ( 1 - σ ǫ | σ | ǫ 29 ( 1 + ǫ | ǫ a R 2 η 1 29 ; τ ) ǫ o ǫ || σ | (1) 8792 J. Phys. Chem. B 2007, 111, 8792-8800 10.1021/jp072686o CCC: $37.00 © 2007 American Chemical Society Published on Web 07/06/2007