Available online at www.sciencedirect.com
ScienceDirect
Materials Today: Proceedings 5 (2018) 20920–20926 www.materialstoday.com/proceedings
2214-7853© 2018 Elsevier Ltd. All rights reserved.
Selection and Peer-review under responsibility of INTERNATIONAL CONFERENCE ON SMART ENGINEERING
MATERIALS (ICSEM 2016).
ICSEM 2016
Development of Electrospinning System for Synthesis of
Polyvinylpyrrolidone Thin Films for Sensor Applications
Amith V
1
,Sridhar R
1
,Gangadhar Angadi
1
,Prajwal D
1
,Mamatha V
1
,
Narasimha Murthy H N
1
[1] Department of Mechanical Engineering, R.V.College of Engineering, Bengaluru
Abstract
Electrospinning is a systematic process of elaborating nanofibers by forcing a polymer fluid through a spinneret by the
application of electric field. Polyvinylpyrrolidone (PVP) is a hydrophilic polymer that has good film formation properties.PVP
thin films are widely used as a sensitive layer in Surface Acoustic Wave (SAW) sensors in order to detect the volatile organic
compounds.The present study was aimed at development of cost effective electrospinning system for production of quality thin
films and parametric optimization. Experimental investigation was performed by electrospinning of PVP considering 7.5wt %,
10wt %,12.5wt %,15wt %,dissolved in Di-MethylFormamide (DMF). The process parameters considered were voltage of 20kV,
flow rate 0.5ml/hr, needle dimension 21 gauge and tip-to-collector distance 100 mm. It was found that concentration of polymer
is a critical factor in controlling the beads formation and fiber diameters although applied voltage and tip-to-collector distance
also influenced the fiber diameter.With increase in concentration of the polymer solution the formation of beads formation
reduced significantly with increase in fiber diameter. The fiber diameter varied between 25.50 nm to 113.84 nm. Minimum fiber
diameter obtained was 25.5 nm whereas the corresponding bead diameter was 647.39 nm for 10 wt % polymer concentration.
Maximum fibre diameter obtained was for 15 wt % polymer concentration with 135.85 nm and the corresponding bead diameter
of 1208.35 nm. Morphological studies of electrospun thin films by Scanning Electron Microscope (SEM) revealed the formation
of fibres in nano dimension, PVP with 10 wt % dissolved in DMF and suitable process parameters can result in nanofibres with
lesser bead formation.
© 2018 Elsevier Ltd. All rights reserved.
Selection and Peer-review under responsibility of INTERNATIONAL CONFERENCE ON SMART ENGINEERING
MATERIALS (ICSEM 2016).
Keywords:Electrospinning, Polyvinylpyrrolidone, polymer concentration, fibre diameter and SEM
* Corresponding author: Sridhar R, Tel.:+919740400717
E-mail address: sridharr@rvce.edu.in