Pharmacology & Pharmacy, 2020, 11, 118-126
https://www.scirp.org/journal/pp
ISSN Online: 2157-9431
ISSN Print: 2157-9423
DOI: 10.4236/pp.2020.116011 Jun. 29, 2020 118 Pharmacology & Pharmacy
Acetylation of Starch Extracted from Rejected
Fruits of Musa × paradisiaca L. to Obtain a
Pharmaceutical Disintegrant
Karla Dumancela
1
, Eduardo Mayorga
1
, Javier Santamaría-Aguirre
1,2*
1
Facultad de Ciencias Químicas, Universidad Central del Ecuador, Quito, Ecuador
2
Instituto de Investigación en Salud Pública y Zoonosis, CIZ, Universidad Central del Ecuador, Quito, Ecuador
Abstract
There are many natural sources to obtain pharmaceutical grade starch, one of
which is banana (Musa × paradisiaca L.); nevertheless, the use of native starch
has certain disadvantages compared to modified starches, whose disintegrat-
ing properties are better. In this study, starch extracted from rejected fruits of
Musa × paradisiaca L., was modified by acetylation, under the following op-
timized experimental conditions: 130 mL acetic anhydride, 3 mL sodium hy-
droxide 50% p/v for each 15 grams of native starch, at 123˚C during 3 hours.
The reaction resulted in a modified green banana starch with twice as much
swelling capacity compared to unmodified (native) starch; acetylation was ve-
rified by infrared spectroscopy and degree of substitution of acetyl groups by
back titration. The dissolution profiles of Ibuprofen tablets made with banana
modified starch and commercial disintegrant, have no differences according
with their similarity factor, f
2
. It is concluded that it is feasible to use green
banana starch modified through acetylation as a pharmaceutical disintegrant.
Keywords
Modified Banana Starch, Acetylation, Swelling Capacity, Disintegrant,
Dissolution Profile
1. Introduction
In Ecuador the pharmaceutical sector invests only 8% of its profits in research,
this low percentage prevents giving added value to locally developed products, in
such a way that approximately 90% of the components of a drug product are
imported. The lack of research and the almost non-existent national production
How to cite this paper: Dumancela, K.,
Mayorga, E. and Santamaría-Aguirre, J. (2020)
Acetylation of Starch Extracted from Rejected
Fruits of Musa × paradisiaca L. to Obtain a
Pharmaceutical Disintegrant. Pharmacology
& Pharmacy, 11, 118-126.
https://doi.org/10.4236/pp.2020.116011
Received: May 22, 2019
Accepted: June 26, 2020
Published: June 29, 2020
Copyright © 2020 by author(s) and
Scientific Research Publishing Inc.
This work is licensed under the Creative
Commons Attribution International
License (CC BY 4.0).
http://creativecommons.org/licenses/by/4.0/
Open Access