Arabian Journal for Science and Engineering
https://doi.org/10.1007/s13369-020-04467-w
RESEARCH ARTICLE-MECHANICAL ENGINEERING
Investigation of Physico-mechanical Behavior, Permeability and Wall
Shear Stress of Porous HA/PMMA Composite Bone Scaffold
Babar Pasha Mahammod
1
· Emon Barua
1
· Payel Deb
1
· Ashish B. Deoghare
1
· Krishna Murari Pandey
1
Received: 4 August 2019 / Accepted: 23 December 2019
© King Fahd University of Petroleum & Minerals 2020
Abstract
Hydroxyapatite (HA)-based composite bone scaffolds are developed using solvent casting particulate leaching technique by
varying the weight percentages of HA from 50 to 70% (w/w) in polymethyl methacrylate matrix. The chemical properties of
the developed scaffolds are investigated by XRD analysis which shows the presence of crystalline HA and traces of β-TCP in
the scaffolds. The microstructure of the scaffolds is studied by the SEM micrographs, which show porous morphology with
an average pore size of 119 ± 18–148 ± 23 μm and a maximum pore size of 148 ± 23 μm for HA 50 scaffold. The highest
porosity of 75 ± 2.0% is recorded for HA 50 scaffold by conducting liquid displacement test and a maximum compressive
strength of 6.26 ± 0.53 MPa is recorded for HA 60 scaffold by performing uniaxial compression test of the scaffolds. The
permeability and wall shear stress (WSS) of the scaffolds are investigated by computational fluid dynamics (CFD). The
CFD analysis is performed in a fluid domain developed by Boolean operations on the CAD model of the scaffold developed
using micro-computed tomography-based 3D image acquisition technique by Mimics V1. Results show that the permeability
increases and WSS decreases with an increase in the porosity of the scaffolds. However, both permeability and WSS obtained
for the developed scaffolds are within the limit prescribed for the growth of bone tissues. It is concluded that scaffolds with
60 wt% of HA exhibit the best combination of porosity, permeability and compressive strength making it suitable for bone
tissue engineering applications.
Keywords Compressive strength · Porosity · Permeability · Wall shear stress · 3D image analysis
1 Introduction
Bone has the capability to regenerate itself and compensate
for any bone loss caused by defects. But the regeneration
capacity is limited to small defects. Larger defects, known
as segmental bone defects (SBDs), cannot be self-healed [1].
Because of this reason, bone is the second most transplanted
tissue after blood [2]. The present approaches for the treat-
ment of SBDs include autografts and allografts. However,
these techniques have been reported with various limitations
which encouraged the use of bone tissue engineering (BTE)
[2, 3]. The aim of BTE is to repair or reconstruct/regenerate
bone defects by combining cells, scaffolds and appropriate
signaling factors [4, 5]. The key challenge in BTE is to fab-
ricate a scaffold that can mimic the host bone structure in
B Emon Barua
imon18enator@gmail.com
1
Department of Mechanical Engineering, National Institute of
Technology Silchar, Silchar, Assam 788010, India
terms of porosity, compressive strength, permeability and
wall shear stress [6].
Porosity percentage is defined as a fraction of void volume
over the total volume of the scaffold. Scaffolds with requisite
porosity enable better cell seeding and migration of the cells,
leading to tissue regeneration [7, 8]. Along with the porosity,
the pore size of the scaffold also has a significant role. A
larger pore size decreases the internal surface area to volume
ratio, which provides more room for better cell attachment,
tissue in-growth and vascularization [9]. In order to act as a
suitable framework for tissue growth, a scaffold should have
a porosity between 60 and 90% [10] with an average pore
size of 100–400 μm[3, 11].
Compressive strength of the scaffolds enables the load-
bearing capability which supports the tissue growth. The
compressive strength of a scaffold is expected to be close
to the native bone to be repaired with a minimum prescribed
range of 1–10 MPa [12]. Nauman et al. [13] reported that
the compressive strength of cancellous bone lies in the range
of 2–12 MPa. Compressive strength primarily depends on
123